Real time synchrotron x-ray diffraction measurements to determine material strength of shocked single crystals following compression and release

doi:https://doi.org/10.1063/1.3187929

Title: Real time synchrotron x-ray diffraction measurements to determine material strength of shocked single crystals following compression and release

Full Record
Other Related Research

Abstract

We present a method to use real time, synchrotron x-ray diffraction measurements to determine the strength of shocked single crystals following compression and release during uniaxial strain loading. Aluminum and copper single crystals shocked along [111] were examined to peak stresses ranging from 2 to 6 GPa. Synchrotron x rays were used to probe the longitudinal lattice strains near the rear free surface (16 and 5 {micro}m depths for Al and Cu, respectively) of the metal crystals following shock compression and release. The 111 diffraction peaks showed broadening indicating a heterogeneous microstructure in the released state. The diffraction peaks also shifted to lower Bragg angles relative to the ambient Bragg angle; the magnitude of the shift increased with increasing impact stress. The Bragg angle shifts and appropriate averaging procedures were used to determine the macroscopic or continuum strength following compression and release. For both crystals, the strengths upon release increased with increasing impact stress and provide a quantitative measure of the strain hardening that occurs in Al(111) and Cu(111) during the shock and release process. Our results for Al(111) are in reasonable agreement with a previous determination based solely on continuum measurements. Two points are noteworthy about the developments presentedmore »« less

Authors:: Turneaure, Stefan J; Gupta, Y M

Publication Date:: 2009-09-15

Research Org.:: Argonne National Lab. (ANL), Argonne, IL (United States)

Sponsoring Org.:: USDOE

OSTI Identifier:: 1005840

Resource Type:: Journal Article

Journal Name:: J. Appl. Phys.

Additional Journal Information:: Journal Volume: 106; Journal Issue: (3) ; 2009; Journal ID: ISSN 0021-8979

Country of Publication:: United States

Language:: ENGLISH

Subject:: 36 MATERIALS SCIENCE; REAL TIME SYSTEMS; X-RAY DIFFRACTION; MONOCRYSTALS; ALUMINIUM; BRAGG REFLECTION; COMPRESSION; COPPER; MICROSTRUCTURE; STRAIN HARDENING; STRESSES; DEPRESSURIZATION

Citation Formats


                    Turneaure, Stefan J, Gupta, Y M, and WSU). Real time synchrotron x-ray diffraction measurements to determine material strength of shocked single crystals following compression and release.  United States: N. p., 2009. 
        Web.  doi:10.1063/1.3187929.

Copy to clipboard


                    Turneaure, Stefan J, Gupta, Y M, & WSU). Real time synchrotron x-ray diffraction measurements to determine material strength of shocked single crystals following compression and release.  United States.  https://doi.org/10.1063/1.3187929

Copy to clipboard


                    Turneaure, Stefan J, Gupta, Y M, and WSU). Tue .  
        "Real time synchrotron x-ray diffraction measurements to determine material strength of shocked single crystals following compression and release".  United States.  https://doi.org/10.1063/1.3187929.

Copy to clipboard


                    
@article{osti_1005840,

  title        = {Real time synchrotron x-ray diffraction measurements to determine material strength of shocked single crystals following compression and release},

  author       = {Turneaure, Stefan J and Gupta, Y M and WSU)},

  abstractNote = {We present a method to use real time, synchrotron x-ray diffraction measurements to determine the strength of shocked single crystals following compression and release during uniaxial strain loading. Aluminum and copper single crystals shocked along [111] were examined to peak stresses ranging from 2 to 6 GPa. Synchrotron x rays were used to probe the longitudinal lattice strains near the rear free surface (16 and 5 {micro}m depths for Al and Cu, respectively) of the metal crystals following shock compression and release. The 111 diffraction peaks showed broadening indicating a heterogeneous microstructure in the released state. The diffraction peaks also shifted to lower Bragg angles relative to the ambient Bragg angle; the magnitude of the shift increased with increasing impact stress. The Bragg angle shifts and appropriate averaging procedures were used to determine the macroscopic or continuum strength following compression and release. For both crystals, the strengths upon release increased with increasing impact stress and provide a quantitative measure of the strain hardening that occurs in Al(111) and Cu(111) during the shock and release process. Our results for Al(111) are in reasonable agreement with a previous determination based solely on continuum measurements. Two points are noteworthy about the developments presented here: Synchrotron x rays are needed because they provide the resolution required for analyzing the data in the released state; the method presented here can be extended to the shocked state but will require additional measurements.},

  doi          = {10.1063/1.3187929},

  url          = {https://www.osti.gov/biblio/1005840},
  journal      = {J. Appl. Phys.},

  issn         = {0021-8979},

  number       = (3) ; 2009,

  volume       = 106,

  place        = {United States},

  year         = {2009},

  month        = {9}

}

Copy to clipboard

Journal Article:

https://doi.org/10.1063/1.3187929

Other availability

Find in Google Scholar

Search WorldCat to find libraries that may hold this journal

Save / Share:

Export Metadata

Save to My Library

Similar records in OSTI.GOV collections:

Real-time, high-resolution x-ray diffraction measurements on shocked crystals at a synchrotron facility

Journal Article Gupta, Y. M. ; Turneaure, Stefan J. ; Perkins, K. ; ... - Review of Scientific Instruments

The Advanced Photon Source (APS) at Argonne National Laboratory was used to obtain real-time, high-resolution x-ray diffraction measurements to determine the microscopic response of shock-compressed single crystals. Disk shaped samples were subjected to plane shock wave compression by impacting them with half-inch diameter, flat-faced projectiles. The projectiles were accelerated to velocities ranging between 300 and 1200 m/s using a compact powder gun designed specifically for use at a synchrotron facility. The experiments were designed to keep the sample probed volume under uniaxial strain and constant stress for a duration longer than the 153.4 ns spacing between x-ray bunches. X-rays frommore »« less
https://doi.org/10.1063/1.4772577
Real-time microstructure of shocked LiF crystals: Use of synchrotron x-rays

Journal Article Turneaure, Stefan J ; Gupta, Y M ; Zimmerman, K ; ... - J. Appl. Phys.

We describe the use of a third generation synchrotron facility to obtain in situ, real-time, x-ray diffraction measurements in plate impact experiments. Subnanosecond duration x-ray pulses were utilized to record diffraction data from pure and magnesium-doped LiF single crystals shocked along the [111] and [100] orientations. The peak stresses were 3.0 GPa for the [111] oriented LiF and between 3.0 and 5.0 GPa for the [100] oriented LiF. For these stresses, shock compression along [111] results in elastic deformation and shock compression along [100] results in elastic-plastic deformation. Because of the quality of the synchrotron x-ray pulses, both shifting andmore »« less
https://doi.org/10.1063/1.3080176
Subnanosecond x-ray diffraction from laser-shocked crystals

Journal Article Wark, J S ; Whitlock, R R ; Hauer, A A ; ... - Physical Review (Section) B: Condensed Matter; (USA)

Multikilobar shocks were launched into single crystals of (111) silicon with a 1-ns pulse (full width at half maximum) of 1.06-{mu}m light at an irradiance of 10{sup 9}--10{sup 10} W cm{sup {minus}2} using the JANUS research laser at Lawrence Livermore National Laboratory. Transient strains on the order of several percent were thus introduced into the crystal. During the compression of the crystal a short (100 ps) intense burst of x-ray line radiation was produced by focusing a second laser beam, synchronous but delayed with respect to the shock-driving beam, onto a solid target. The x rays were Bragg diffracted frommore »« less
https://doi.org/10.1103/PhysRevB.40.5705
Calibration of NRSF2 Instrument at HFIR

Technical Report Tang, Fei ; Hubbard, Camden R

The Neutron Residual Stress Mapping Facility (NRSF2) at HB-2B is a new generation-diffraction instrument, adding many new Second Generation features, such as larger beam tube, large sample XYZ goniometer, and KAPPA orienter for a broad range of materials behavior studies. One key feature is the NRSF2 monochromator, which is a double focusing, double crystal monochromator system consisting of two sets of stacked Si crystal wafers. One set of wafers has Si[400] plane normal to the surface while the other set of wafers has the Si[500] normal to the surface. The monochromator crystal diffracts at a fixed diffraction angle of 88{supmore »« less
https://doi.org/10.2172/969651

Full Text Available
Strength and deformation of shocked diamond single crystals: Orientation dependence

Journal Article Lang, John Michael Jr. ; Winey, J. M. ; Gupta, Y. M. - Physical Review B

Understanding and quantifying the strength or elastic limit of diamond single crystals is of considerable scientific and technological importance, and has been a subject of long standing theoretical and experimental interest. To examine the effect of crystalline anisotropy on strength and deformation of shocked diamond single crystals, plate impact experiments were conducted to measure wave profiles at various elastic impact stresses up to ~120 GPa along [110] and [111] crystal orientations. Using laser interferometry, particle velocity histories and shock velocities in the diamond samples were measured and were compared with similar measurements published previously for shock compression along the [100]more »« less
https://doi.org/10.1103/PhysRevB.97.104106

Full Text Available

Similar Records