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Title: Sulfur removal from high-sulfur Illinois coal by low-temperature perchloroethylene (PCE) extraction. Technical report, December 1, 1991--February 29, 1992

Technical Report ·
DOI:https://doi.org/10.2172/10172071· OSTI ID:10172071
; ; ; ; ; ; ; ;  [1];  [2];  [3]; ;  [4]
  1. Illinois State Geological Survey, Champaign, IL (United States)
  2. Eastern Illinois Univ., Charleston, IL (United States)
  3. Illinois Univ., Urbana, IL (United States)
  4. Kentucky Univ., Lexington, KY (United States)

A pre-combustion coal desulfurization process at 120{degree}C using perchloroethylene (PCE) to remove up to 70% of the organic sulfur has been developed by the Midwest Ore Processing Co. (MWOPC). However, this process has not yet proven to be as successful with Illinois coals as it has for Ohio and Indiana coals. In addition, the high levels of organic sulfur removals observed by the MWOPC may be due to certain errors involved in the ASTM data interpretation; this needs verification. For example, elemental sulfur extracted by the PCE may be derived from pyrite oxidation during coal preoxidation, but it may be interpreted as organic sulfur removed by the PCE using ASTM analysis. The purposes of this research are to independently confirm and possibly to improve the organic sulfur removal from Illinois coals with the PCE desulfurization process reported by the MWOPC and to verify the forms-of-sulfur determination using the ASTM method for the PCE process evaluation.

Research Organization:
Illinois State Geological Survey, Champaign, IL (United States)
Sponsoring Organization:
USDOE, Washington, DC (United States); Illinois Dept. of Energy and Natural Resources, Springfield, IL (United States)
DOE Contract Number:
FG22-91PC91334
OSTI ID:
10172071
Report Number(s):
DOE/PC/91334-T57; ON: DE92018296
Resource Relation:
Other Information: PBD: [1992]
Country of Publication:
United States
Language:
English