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Title: COST-EFFECTIVE METHOD FOR PRODUCING SELF SUPPORTED PALLADIUM ALLOY MEMBRANES FOR USE IN EFFICIENT PRODUCTION OF COAL DERIVED HYDROGEN

Technical Report ·
DOI:https://doi.org/10.2172/894522· OSTI ID:894522

In the past quarter, we have conducted additional characterization and permeation tests on different Pd alloy membranes including PdCuTa ternary alloy materials. We attempted to address some discrepancies between SwRI{reg_sign} and CSM relating to PdCu stoichiometry by preparing a range of PdCu membranes with compositions from {approx}58-65 at% Pd (bal. Cu). While some difficulties in cutting and sealing these thin membranes at CSM continue, some progress has been made in identifying improved membrane support materials. We have also completed an initial cost analysis for large-scale vacuum deposition and fabrication of thin Pd ally membranes and project that the process can meet DOE cost targets. Minimal progress was made in the past quarter relating to the testing of prototype membrane modules at Idatech. In the past quarter Idatech was acquired by a UK investment firm, which we believe may have impacted the ability of key technical personnel to devote sufficient time to support this effort. We are hopeful their work can be completed by the end of the calendar year.

Research Organization:
Southwest Research Institute Inc
Sponsoring Organization:
USDOE
DOE Contract Number:
FC26-03NT41849
OSTI ID:
894522
Country of Publication:
United States
Language:
English