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Title: Miniature Mass Spectrometers for Hydrogen Isotopic Analyses

Technical Report ·
DOI:https://doi.org/10.2172/811368· OSTI ID:811368

As part of the Defense Programs Plant Directed Research and Development Program, the Savannah River Technology Center investigated the emerging area of miniature mass sensors for hydrogen and hydrogen isotope analysis. New sensors from Ferran Scientific and a beta prototype sensor from Mass Sensors, Inc. were purchased. A small pumping platform was designed and assembled. Components for miniature ion traps were investigated based on design information from Oak Ridge National Laboratories. The systems were compared to a conventional residual gas analyzer based on a Stanford Research RGA 300. Each of the sensors investigated had distinct advantages for particular applications. The Ferran system was the least expensive and the smallest, but it had low resolution for hydrogen and deuterium mixtures. The Mass Sensor unit used a new ExB design which achieved excellent resolution of the hydrogen isotopes in a small package. One limitation with the current design was the small 3 to 4 order dynamic range and another was a need for a variable sampling rate to speed analysis over a wider mass range.

Research Organization:
Savannah River Site (SRS), Aiken, SC (United States)
Sponsoring Organization:
US Department of Energy (US)
DOE Contract Number:
AC09-96SR18500
OSTI ID:
811368
Report Number(s):
WSRC-TR-2002-00554; TRN: US200311%%372
Resource Relation:
Other Information: PBD: 29 May 2003
Country of Publication:
United States
Language:
English