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Title: Evaluation of polyaryl adhesives in elastomer-stainless steel joints

Technical Report ·
DOI:https://doi.org/10.2172/6631160· OSTI ID:6631160

Polyaryl thermoplastic adhesives (polyetheretherketone, PEEK, polyphenylene sulfide PPS, polyphenylethersulfone, PES) were evaluated for ability to bond elastomer to metal for use in geothermal environments. Strength of elastomer-to-metal joints adhesives blends (such as in drill pipe or casing protectors) were determined using peel tests. Parameters involved in making the joints were temperature, time and atmosphere, in addition to type of adhesive. Physical chemical analyses have aided endeavors to determine the cause of adhesion failure in the joint: differential thermal analyses, thermal gravimetric analyses, infrared spectroscopy and electron spectroscopy for chemical analysis. Tests showed that joints made of adhesive blends which contained greater than 50% PES survived simulated geothermal conditions (200C, water vapor pressure 200 psi) for weeks without significant decrease in peel strength. Chemical components of the adhesive appear to be highly stable under the conditions required to make the joints and in subsequent exposure to the simulated geothermal environment.

Research Organization:
Brookhaven National Lab. (BNL), Upton, NY (United States)
Sponsoring Organization:
USDOE; USDOE, Washington, DC (United States)
DOE Contract Number:
AC02-76CH00016
OSTI ID:
6631160
Report Number(s):
BNL-48089; ON: DE93009794
Country of Publication:
United States
Language:
English