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Title: Sensitization of Parker fittings

Technical Report ·
DOI:https://doi.org/10.2172/6490506· OSTI ID:6490506

At your request, ferrules from 316 SS Parker-Hannifen compression fittings at the FFTF have been examined and evaluated to determine the metallurgical condition as related to carbide precipitation in grain boundaries (known as sensitization) and the implications this may have with regard to corrosion resistance. To accomplish this, two ferrules from new stock, two ferrules from old stock and two ferrules that had seen service were examined metallurgically. The samples were prepared for optical metallography. They were viewed in both the etched and unetched condition and analyzed on the scanning electron microscope (SEM) for elemental content. It was confirmed that the ferrules from new stock had a 5 mil thick nitrided layer on the ferrule ID at the lead end and that the 316 SS ferrule material was in the sensitized condition, indicating low resistance to aqueous corrosion. The material from old stock had no nitride layer but was in the sensitized condition indicating low resistance to aqueous corrosion. The ferrules that had seen service had not been nitrided and were not sensitized indicating high resistance to aqueous corrosion.

Research Organization:
Hanford Engineering Development Lab., Richland, WA (United States)
DOE Contract Number:
AC06-76FF02170
OSTI ID:
6490506
Report Number(s):
HEDL-7553; ON: DE85018506
Country of Publication:
United States
Language:
English