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Title: Investigation of reactivity between SiC and Nb-1Zr in planned irradiation creep experiments

Technical Report ·
DOI:https://doi.org/10.2172/543203· OSTI ID:543203

Thermodynamic calculations and diffusion couple experiments showed that SiC and Nb-1Zr were reactive at the upper range of temperatures anticipated in the planned irradiation creep experiment. Sputter-deposited aluminum oxide (Al{sub 2}O{sub 3}) was selected as a diffusion barrier coating. Experiments showed that although the coating coarsened at high temperature it was an effective barrier for diffusion of silicon from SiC into Nb-1Zr. Therefore, to avoid detrimental reactions between the SiC composite and the Nb-1Zr pressurized bladder during the planned irradiation creep experiment, a coating of Al{sub 2}O{sub 3} will be required on the Nb-1Zr bladder.

Research Organization:
Oak Ridge National Lab. (ORNL), Oak Ridge, TN (United States)
DOE Contract Number:
AC06-76RL01830
OSTI ID:
543203
Report Number(s):
DOE/ER-0313/22; ON: DE97008797; TRN: 97:020242
Resource Relation:
Other Information: PBD: Aug 1997; Related Information: Is Part Of Fusion materials semiannual progress report for period ending June 30, 1997; PB: 358 p.
Country of Publication:
United States
Language:
English