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Title: Role of temperature, solvent and agitation in coal dissolution and liquefaction. Quarterly report, December 1981-February 1982

Technical Report ·
DOI:https://doi.org/10.2172/5384095· OSTI ID:5384095

A Plexiglas reactor was constructed and experiments carried out with three mixer configurations in a sand-water system to determine the best mixer configuration and the minimum rpm to produce uniform conditions during coal dissolution. Coal dissolution experiments on Kentucky No. 9 coal were made with combinations of tetralin and 2-methylnaphthalene to obtain the optimum ratio in the solvent. The effect of ..beta..-naphthol addition to the solvent on the dissolution of Kentucky No. 9 coal was studied. The effect of holding time at 400/sup 0/C on the dissolution of Kentucky No. 9 coal in a solvent containing 46.1 wt % tetralin, 46.1 wt % 2-methylnaphthalene, 2.9 wt % ..gamma..-picoline and 4.9 wt % ..beta..-naphthol was studied.

Research Organization:
Michigan Univ., Ann Arbor (USA). Dept. of Chemical Engineering
DOE Contract Number:
FG22-81PC40811
OSTI ID:
5384095
Report Number(s):
DOE/PC/40811-2; ON: DE82013413
Country of Publication:
United States
Language:
English