skip to main content
OSTI.GOV title logo U.S. Department of Energy
Office of Scientific and Technical Information

Title: Investigation of the silicon loss in APS MoSi{sub 2} under the range of typical spray conditions

Technical Report ·
DOI:https://doi.org/10.2172/373893· OSTI ID:373893
; ;  [1];  [2]
  1. Los Alamos National Lab., NM (United States)
  2. Sandia National Labs., Albuquerque, NM (United States)

MoSi{sub 2} provides good high temperature oxidation and corrosion resistance. However, the lower silicides such as Mo{sub 5}Si{sub 3} do not provide such resistance. In this study, air plasma sprayed (APS) MoSi{sub 2} particle temperatures and velocities were measured under various torch conditions chosen to span the majority of typically utilized spray parameters. Empirical models of particle temperature and velocity were computed from the data. Three spray conditions were chosen to produce high, medium and low particle temperature and velocities. Coatings produced under these spray conditions were characterized by profile tracing, quantitative x-ray diffraction, and SEM analysis. The Mo{sub 5}Si{sub 3} level in the coatings ranged from 5% to 8% while the Mo{sub 5}Si{sub 3} level in the starting powder was 0.6%. Particle size, particle trajectory, and torch parameters were found to be important factors in the Si loss process when APS depositing MoSi{sub 2}.

Research Organization:
Los Alamos National Lab. (LANL), Los Alamos, NM (United States)
Sponsoring Organization:
USDOE, Washington, DC (United States)
DOE Contract Number:
W-7405-ENG-36
OSTI ID:
373893
Report Number(s):
LA-UR-96-1805; CONF-961009-4; ON: DE96011613; TRN: 96:024908
Resource Relation:
Conference: 9. national thermal spray conference and exposition, Cincinnati, OH (United States), 7-11 Oct 1996; Other Information: PBD: [1996]
Country of Publication:
United States
Language:
English