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Title: Preparation of Pu{sup 239} sources

Technical Report ·
DOI:https://doi.org/10.2172/353213· OSTI ID:353213

The Separations Technology Laboratory has prepared four sources to be used for calibrating a waste assay system (Passive/Active Neutron Assay) in Building 724-8G (Burial Ground). The four sources contain 0.5, 0.1, 0.05, and 0.01 grams Pu{sup 239}, respectively. The sources were prepared using aliquots from a single solution provided by the Quality Control (QC) group of Laboratories Department. The solution contained weapons-grade plutonium dissolved in nitric acid. Final solution acidity was 3M. Coulometry had been used to obtain a total plutonium content per unit volume. The weight percent of the plutonium isotopes present was obtained via mass spectrometry.

Research Organization:
E.I. du Pont de Nemours and Co., Savannah River Plant, Aiken, SC (United States)
Sponsoring Organization:
USDOE, Washington, DC (United States)
DOE Contract Number:
AC09-89SR18035; AC09-76SR00001
OSTI ID:
353213
Report Number(s):
DPSP-88-272-84; ON: DE99002881; TRN: AHC29923%%44
Resource Relation:
Other Information: PBD: 5 Aug 1988
Country of Publication:
United States
Language:
English