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Title: Synthesis of novel ionic liquids from lignin-derived compounds

Patent ·
OSTI ID:1393557

Methods and compositions are provided for synthesizing ionic liquids from lignin derived compounds comprising: contacting a starting material comprising lignin with a depolymerization agent to depolymerize the lignin and form a mixture of aldehyde containing compounds; contacting the mixture of aldehyde containing compounds with an amine under conditions suitable to convert the mixture of aldehyde containing compounds to a mixture of amine containing compounds; and contacting the mixture of amine containing compounds with an acid under conditions suitable to form an ammonium salt, thereby preparing the ionic liquid.

Research Organization:
Lawrence Berkeley National Laboratory (LBNL), Berkeley, CA (United States)
Sponsoring Organization:
USDOE
DOE Contract Number:
AC02-05CH11231
Assignee:
The Regents of the University of California
Patent Number(s):
9,765,044
Application Number:
14/776,454
OSTI ID:
1393557
Resource Relation:
Patent File Date: 2014 Mar 14
Country of Publication:
United States
Language:
English

References (2)

Product preparation and recovery from thermolysis of lignocellulosics in ionic liquids patent-application August 2008
Reductive Amination of Aldehydes and Ketones with Sodium Triacetoxyborohydride. Studies on Direct and Indirect Reductive Amination Procedures journal January 1996