Large-surface-area diamond (111) crystal plates for applications in high-heat-load wavefront-preserving X-ray crystal optics

Stoupin, Stanislav; Antipov, Sergey; Butler, James E.; Kolyadin, Alexander V.; Katrusha, Andrey

doi:10.1107/S1600577516011796

Title: Large-surface-area diamond (111) crystal plates for applications in high-heat-load wavefront-preserving X-ray crystal optics

Journal Article · Wed Aug 10 00:00:00 EDT 2016 · Journal of Synchrotron Radiation (Online)

DOI:https://doi.org/10.1107/S1600577516011796· OSTI ID:1392112

Stoupin, Stanislav ^[1]; Antipov, Sergey ^[2]; Butler, James E. ^[2]; Kolyadin, Alexander V. ^[3]; Katrusha, Andrey ^[3]

Argonne National Lab. (ANL), Argonne, IL (United States)
Euclid Techlabs LLC, Solon, OH (United States)
New Diamond Technology LLC, St. Petersburg (Russia)

Fabrication and results of high-resolution X-ray topography characterization of diamond single-crystal plates with large surface area (10 mm × 10 mm) and (111) crystal surface orientation for applications in high-heat-load X-ray crystal optics are reported. The plates were fabricated by laser-cutting of the (111) facets of diamond crystals grown using high-pressure high-temperature methods. The intrinsic crystal quality of a selected 3 mm × 7 mm crystal region of one of the studied samples was found to be suitable for applications in wavefront-preserving high-heat-load crystal optics. Wavefront characterization was performed using sequential X-ray diffraction topography in the pseudo plane wave configuration and data analysis using rocking-curve topography. In conclusion, the variations of the rocking-curve width and peak position measured with a spatial resolution of 13 µm × 13 µm over the selected region were found to be less than 1 µrad.

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Research Organization:: Argonne National Lab. (ANL), Argonne, IL (United States)

Sponsoring Organization:: USDOE Office of Science (SC), Basic Energy Sciences (BES) (SC-22), Scientific User Facilities Division; Argonne National Laboratory, Advanced Photon Source

Grant/Contract Number:: AC02-06CH11357

OSTI ID:: 1392112

Journal Information:: Journal of Synchrotron Radiation (Online), Vol. 23, Issue 5; ISSN 1600-5775

Publisher:: International Union of CrystallographyCopyright Statement

Country of Publication:: United States

Language:: English

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Cited by: 8 works

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References (14)

μm-resolved high resolution X-ray diffraction imaging for semiconductor quality control Lübbert, D.; Baumbach, T.; Härtwig, J. Nuclear Instruments and Methods in Physics Research Section B: Beam Interactions with Materials and Atoms, Vol. 160, Issue 4 https://doi.org/10.1016/S0168-583X(99)00619-9	journal	April 2000
Goniometric and topographic characterization of synthetic IIa diamonds Tamasaku, Kenji; Ueda, Tomoyasu; Miwa, Daigo Journal of Physics D: Applied Physics, Vol. 38, Issue 10A https://doi.org/10.1088/0022-3727/38/10A/012	journal	May 2005
Test of a high-heat-load double-crystal diamond monochromator at the Advanced Photon Source Fernandez, P. B.; Graber, T.; Lee, W. -K Nuclear Instruments and Methods in Physics Research Section A: Accelerators, Spectrometers, Detectors and Associated Equipment, Vol. 400, Issue 2-3 https://doi.org/10.1016/S0168-9002(97)01014-0	journal	December 1997
Multiple station beamline at an undulator X-ray source Als-Nielsen, J.; Freund, A. K.; Grübel, G. Nuclear Instruments and Methods in Physics Research Section B: Beam Interactions with Materials and Atoms, Vol. 94, Issue 3 https://doi.org/10.1016/0168-583X(94)95370-8	journal	November 1994
A simple model to describe the anisotropy of diamond polishing van Bouwelen, F. M.; van Enckevort, W. J. P. Diamond and Related Materials, Vol. 8, Issue 2-5 https://doi.org/10.1016/S0925-9635(98)00347-1	journal	March 1999
Performance of a beam-multiplexing diamond crystal monochromator at the Linac Coherent Light Source Zhu, Diling; Feng, Yiping; Stoupin, Stanislav Review of Scientific Instruments, Vol. 85, Issue 6, Article No. 063106 https://doi.org/10.1063/1.4880724	journal	June 2014
Large Defect-Free Synthetic Type IIa Diamond Crystals Synthesized via High Pressure and High Temperature Sumiya, Hitoshi; Tamasaku, Kenji Japanese Journal of Applied Physics, Vol. 51, Issue 9R https://doi.org/10.7567/JJAP.51.090102	journal	September 2012
Strain mapping with parts-per-million resolution in synthetic type-Ib diamond plates Macrander, Albert T.; Krasnicki, Szczesny; Zhong, Yuncheng Applied Physics Letters, Vol. 87, Issue 19 https://doi.org/10.1063/1.2126790	journal	November 2005
Diamond double-crystal monochromator at SPring-8 Goto, S.; Yamazaki, H.; Shimizu, Y. SPIE Optical Engineering + Applications, SPIE Proceedings https://doi.org/10.1117/12.932287	conference	October 2012
HPHT growth and x-ray characterization of high-quality type IIa diamond Burns, R. C.; Chumakov, A. I.; Connell, S. H. Journal of Physics: Condensed Matter, Vol. 21, Issue 36 https://doi.org/10.1088/0953-8984/21/36/364224	journal	August 2009
All-diamond optical assemblies for a beam-multiplexing X-ray monochromator at the Linac Coherent Light Source Stoupin, S.; Terentyev, S. A.; Blank, V. D. Journal of Applied Crystallography, Vol. 47, Issue 4, p. 1329-1336 https://doi.org/10.1107/S1600576714013028	journal	August 2014
Diamond Double-Crystal Monochromator for SPring-8 Undulator Beamlines Yabashi, M.; Goto, S.; Shimizu, Y. SYNCHROTRON RADIATION INSTRUMENTATION: Ninth International Conference on Synchrotron Radiation Instrumentation, AIP Conference Proceedings https://doi.org/10.1063/1.2436212	conference	January 2007
Diamond crystal optics for self-seeding of hard X-rays in X-ray free-electron lasers Stoupin, S.; Blank, V. D.; Terentyev, S. A. Diamond and Related Materials, Vol. 33, p. 1-4 https://doi.org/10.1016/j.diamond.2012.12.009	journal	March 2013
A diamond double‐crystal transmission monochromator for the TROIKA II station at ESRF Grübel, G.; Abernathy, D.; Vignaud, G. Review of Scientific Instruments, Vol. 67, Issue 9 https://doi.org/10.1063/1.1147490	journal	September 1996

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46 INSTRUMENTATION RELATED TO NUCLEAR SCIENCE AND TECHNOLOGY
X-ray monochromator
high heat load
diamond crystal
wavefront preservation

Title: Large-surface-area diamond (111) crystal plates for applications in high-heat-load wavefront-preserving X-ray crystal optics

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