Method of making alkali metal hydrides

Pecharsky, Vitalij K.; Gupta, Shalabh; Pruski, Marek; Hlova, Ihor; Castle, Andra

Title: Method of making alkali metal hydrides

Patent · Tue May 30 00:00:00 EDT 2017

OSTI ID:1360969

Pecharsky, Vitalij K.; Gupta, Shalabh; Pruski, Marek; Hlova, Ihor; Castle, Andra

A method is provided for making alkali metal hydrides by mechanochemically reacting alkali metal and hydrogen gas under mild temperature (e.g room temperature) and hydrogen pressure conditions without the need for catalyst, solvent, and intentional heating or cooling.

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Research Organization:: Ames Laboratory (AMES), Ames, IA (United States)

Sponsoring Organization:: USDOE

DOE Contract Number:: AC02-07CH11358

Assignee:: Iowa State University Research Foundation, Inc.

Patent Number(s):: 9,663,364

Application Number:: 14/757,132

OSTI ID:: 1360969

Resource Relation:: Patent File Date: 2015 Nov 23

Country of Publication:: United States

Language:: English

References (10)

Process of Manufacture of Alkali-Metal Hydrides Freudenberg, Hermann; Kloepfer, Harry https://doi.org/https://image-ppubs.uspto.gov/dirsearch-public/print/downloadPdf/1796265 US Patent Document 1,796,265	patent	March 1931
Production of Alkali Metal Hydride Hansley, Virgil L. https://doi.org/https://image-ppubs.uspto.gov/dirsearch-public/print/downloadPdf/2372670 US Patent Document 2,372,670	patent	April 1945
Production of Alkali Metal Hydride Hansley, Virgil L. https://doi.org/https://image-ppubs.uspto.gov/dirsearch-public/print/downloadPdf/2372671 US Patent Document 2,372,671	patent	April 1945
Process for Preparing Sodium Hydride Hansley, VIrgil L.; Morgan, Fred Keith https://doi.org/https://image-ppubs.uspto.gov/dirsearch-public/print/downloadPdf/3222288 US Patent Document 3,222,288	patent	December 1965
Preparation of Alkaline Earth Metal Aluminum Hydrides Snyder, John C. https://doi.org/https://image-ppubs.uspto.gov/dirsearch-public/print/downloadPdf/3387948 US Patent Document 3,387,948	patent	June 1968
Preparation of Metal Hydrides Snyder, John C. https://doi.org/https://image-ppubs.uspto.gov/dirsearch-public/print/downloadPdf/3387949 US Patent Document 3,387,949	patent	June 1968
Preparation of Metal Hydrides Snyder, John C. https://doi.org/https://image-ppubs.uspto.gov/dirsearch-public/print/downloadPdf/3485585 US Patent Document 3,485,585	patent	December 1969
Preparation of the hydrides Mg2FeH6 and Mg2CoH5 by mechanical alloying followed by sintering Huot, J.; Hayakawa, H.; Akiba, E. Journal of Alloys and Compounds, Vol. 248, Issue 1-2 https://doi.org/10.1016/S0925-8388(96)02705-3	journal	February 1997
Preparation of alkali metal hydrides by mechanical alloying Elansari, L.; Antoine, L.; Janot, R. Journal of Alloys and Compounds, Vol. 329, Issue 1-2 https://doi.org/10.1016/S0925-8388(01)01615-2	journal	November 2001
Hydrogenation properties of complex alkali metal hydrides fabricated by mechano-chemical synthesis Zaluski, L.; Zaluska, A.; Ström-Olsen, J. O. Journal of Alloys and Compounds, Vol. 290, Issue 1-2 https://doi.org/10.1016/S0925-8388(99)00211-X	journal	August 1999

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