Transmission-geometry electrochemical cell for in-situ scattering and spectroscopy investigations

Chupas, Peter J.; Chapman, Karena W.; Kurtz, Charles A.; Borkiewicz, Olaf J.; Wiaderek, Kamila Magdelena; Shyam, Badri

Title: Transmission-geometry electrochemical cell for in-situ scattering and spectroscopy investigations

Patent · Tue May 05 00:00:00 EDT 2015

OSTI ID:1347439

Chupas, Peter J.; Chapman, Karena W.; Kurtz, Charles A.; Borkiewicz, Olaf J.; Wiaderek, Kamila Magdelena; Shyam, Badri

The present invention relates to a test chamber that can be used to perform a variety of X-ray and neutron spectroscopy experiments including powder diffraction, small-angle scattering, X-ray absorption spectroscopy, and pair distribution functions, such chamber comprising a first electrode with an X-ray transparent window; a second electrode with an X-ray transparent window; a plurality of insulating gaskets providing a hermetic seal around the sample and preventing contact between said first and second electrodes; and an insulating housing into which the first electrode is secured.

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Research Organization:: Argonne National Laboratory (ANL), Argonne, IL (United States)

Sponsoring Organization:: USDOE

DOE Contract Number:: AC02-06CH11357

Assignee:: UChicago Argonne, LLC (Chicgo, IL)

Patent Number(s):: 9,022,652

Application Number:: 13/631,207

OSTI ID:: 1347439

Resource Relation:: Patent File Date: 2012 Sep 28

Country of Publication:: United States

Language:: English

References (6)

Sample cell support assembly for fluorescent X-ray analysis Mizuta, Masao https://doi.org/https://image-ppubs.uspto.gov/dirsearch-public/print/downloadPdf/5253280 US Patent Document 5,253,280	patent	October 1993
Apparatus for in situ x-ray study of electrochemical cells Amatucci, Glenn G.; Tarascon, Jean-Marie https://doi.org/https://image-ppubs.uspto.gov/dirsearch-public/print/downloadPdf/5635138 US Patent Document 5,635,138	patent	June 1997
Compact X-ray spectrometer Golenhofen, Rainer https://doi.org/https://image-ppubs.uspto.gov/dirsearch-public/print/downloadPdf/6233307 US Patent Document 6,233,307	patent	May 2001
System structure for in situ x-ray study of electrochemical cell component performance Gural, John A.; Leriche, Jean-Bernard; Morcrette, Mathieu https://doi.org/https://image-ppubs.uspto.gov/dirsearch-public/print/downloadPdf/7022290 US Patent Document 7,022,290	patent	April 2006
Pre-filmed precision sample cell for x-ray analyzer Burdett, Jr., John H.; Dunham, Daniel; Quinn, James B. https://doi.org/https://image-ppubs.uspto.gov/dirsearch-public/print/downloadPdf/7729471 US Patent Document 7,729,471	patent	June 2010
A compact high vacuum heating chamber for in-situ x-ray scattering studies Bertram, F.; Deiter, C.; Pflaum, K. Review of Scientific Instruments, Vol. 83, Issue 8 https://doi.org/10.1063/1.4746290	journal	August 2012

Cited By (1)

Transmission-geometry electrochemical cell for in-situ scattering and spectroscopy investigations Chupas, Peter J.; Chapman, Karena; Kurtz, Charles A. https://doi.org/https://image-ppubs.uspto.gov/dirsearch-public/print/downloadPdf/9022652 US Patent Document 9,022,652	patent	May 2015

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Title: Transmission-geometry electrochemical cell for in-situ scattering and spectroscopy investigations

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