Advancing polymers of intrinsic microporosity by mechanochemistry

Zhang, Pengfei; Jiang, Xueguang; Wan, Shun; Dai, Sheng

doi:10.1039/C4TA07196D

Title: Advancing polymers of intrinsic microporosity by mechanochemistry

Journal Article · Fri Feb 20 00:00:00 EST 2015 · Journal of Materials Chemistry. A

DOI:https://doi.org/10.1039/C4TA07196D· OSTI ID:1265468

Zhang, Pengfei ^[1]; Jiang, Xueguang ^[2]; Wan, Shun ^[1]; Dai, Sheng ^[3]

Oak Ridge National Laboratory (ORNL), Oak Ridge, TN (United States)
Univ. of Tennessee, Knoxville, TN (United States)
Oak Ridge National Laboratory (ORNL), Oak Ridge, TN (United States); Univ. of Tennessee, Knoxville, TN (United States)

Herein, we report a fast (15 min) and solvent-free mechanochemical approach to construct polymers of intrinsic microporosity (PIMs) with high molecular mass and low polydispersity by solid grinding. The enhanced reaction efficiency results from the instantaneous frictional heating and continuous exposure of active sites within those solid reactants.

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Research Organization:: Oak Ridge National Lab. (ORNL), Oak Ridge, TN (United States); Energy Frontier Research Centers (EFRC) (United States). Fluid Interface Reactions, Structures and Transport Center (FIRST)

Sponsoring Organization:: USDOE Office of Science (SC), Basic Energy Sciences (BES)

Grant/Contract Number:: AC05-00OR22725

OSTI ID:: 1265468

Journal Information:: Journal of Materials Chemistry. A, Vol. 3, Issue 13; ISSN 2050-7488

Publisher:: Royal Society of ChemistryCopyright Statement

Country of Publication:: United States

Language:: English

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Cited by: 41 works

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Entropy-Driven Mechanochemical Synthesis of Polymetallic Zeolitic Imidazolate Frameworks for CO ₂ Fixation Xu, Wei; Chen, Hao; Jie, Kecheng Angewandte Chemie International Edition, Vol. 58, Issue 15 https://doi.org/10.1002/anie.201900787	journal	March 2019
Mechanochemical Synthesis of Ruthenium Cluster@Ordered Mesoporous Carbon Catalysts by Synergetic Dual Templates Wang, Li; Zhao, Jiahua; Zhang, Pengfei Chemistry – A European Journal, Vol. 25, Issue 36 https://doi.org/10.1002/chem.201901714	journal	May 2019
The Effect of Thermal Treatment on the Hydrogen‐Storage Properties of PIM‐1 Ramimoghadam, Donya; Boyd, Sue E.; Brown, Christopher L. ChemPhysChem, Vol. 20, Issue 12 https://doi.org/10.1002/cphc.201900222	journal	May 2019
The synthesis of polymers of intrinsic microporosity (PIMs) McKeown, Neil B. Science China Chemistry, Vol. 60, Issue 8 https://doi.org/10.1007/s11426-017-9058-x	journal	July 2017
Coordination-supported organic polymers: mesoporous inorganic–organic materials with preferred stability Chen, Dong; Zhang, Pengfei; Fang, Qianrong Inorganic Chemistry Frontiers, Vol. 5, Issue 8 https://doi.org/10.1039/c8qi00471d	journal	January 2018
Solvent-free and rapid synthesis of mesoporous Pt–iron oxide catalysts via mechanochemical assembly Zhou, Min; Zhao, Jiahua; Zhang, Pengfei Catalysis Science & Technology, Vol. 9, Issue 15 https://doi.org/10.1039/c9cy00970a	journal	January 2019
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