Sub-Kelvin magnetic and electrical measurements in a diamond anvil cell with in-situ tunability

Palmer, Alexander; Silevitch, Daniel; Feng, Yejun; Wang, Yishu; Jaramillo, R.; Banerjee, Arnab; Ren, Yang; Rosenbaum, Thomas F.

doi:10.1063/1.4929861

Title: Sub-Kelvin magnetic and electrical measurements in a diamond anvil cell with in-situ tunability

Journal Article · Fri Sep 04 00:00:00 EDT 2015 · Review of Scientific Instruments

DOI:https://doi.org/10.1063/1.4929861· OSTI ID:1224169

Palmer, Alexander ^[1]; Silevitch, Daniel ^[1]; Feng, Yejun ^[2]; Wang, Yishu ^[1]; Jaramillo, R. ^[3]; Banerjee, Arnab ^[4]; Ren, Yang ^[5]; Rosenbaum, Thomas F. ^[6]

Univ. of Chicago, IL (United States)
Univ. of Chicago, IL (United States); Argonne National Lab. (ANL), Argonne, IL (United States)
Massachusetts Inst. of Technology (MIT), Cambridge, MA (United States)
Oak Ridge National Lab. (ORNL), Oak Ridge, TN (United States)
Argonne National Lab. (ANL), Argonne, IL (United States)
Univ. of Chicago, IL (United States); California Inst. of Technology (CalTech), Pasadena, CA (United States)

We discuss techniques for performing continuous measurements across a wide range of pressure-field-temperature phase space, combining the milli-Kelvin temperatures of a helium dilution refrigerator with that of the giga-Pascal pressures of a diamond anvil cell and the Tesla magnetic fields of a superconducting magnet. With a view towards minimizing remnant magnetic fields and background magnetic susceptibility, we then characterize high-strength superalloy materials for the pressure cell assembly, which allows high fidelity measurements of low-field phenomena such as superconductivity below 100 mK at pressures above 10 GPa. In situ tunability and measurement of the pressure permit experiments over a wide range of pressure, while at the same time making possible precise steps across abrupt phase transitions such as that from insulator to metal.

View Accepted Manuscript (DOE)

Cite

Export

Save

Research Organization:: Oak Ridge National Laboratory (ORNL), Oak Ridge, TN (United States)

Sponsoring Organization:: USDOE Office of Science (SC)

Grant/Contract Number:: AC05-00OR22725

OSTI ID:: 1224169

Journal Information:: Review of Scientific Instruments, Vol. 86, Issue 9; ISSN 0034-6748

Publisher:: American Institute of Physics (AIP)Copyright Statement

Country of Publication:: United States

Language:: English

Citation Metrics:

Cited by: 6 works

Citation information provided by
Web of Science

References (57)

Formation of a Nematic Fluid at High Fields in Sr3Ru2O7 Borzi, R. A.; Grigera, S. A.; Farrell, J. Science, Vol. 315, Issue 5809 https://doi.org/10.1126/science.1134796	journal	January 2007
Superconductivity without phonons Monthoux, P.; Pines, D.; Lonzarich, G. G. Nature, Vol. 450, Issue 7173 https://doi.org/10.1038/nature06480	journal	December 2007
Ferroelectric quantum criticality Rowley, S. E.; Spalek, L. J.; Smith, R. P. Nature Physics, Vol. 10, Issue 5 https://doi.org/10.1038/nphys2924	journal	March 2014
Pressure Induced Superconductivity in Pristine $1 T − {TiSe}_{2}$ Kusmartseva, A. F.; Sipos, B.; Berger, H. Physical Review Letters, Vol. 103, Issue 23 https://doi.org/10.1103/PhysRevLett.103.236401	journal	November 2009
Signatures of quantum criticality in pure Cr at high pressure Jaramillo, R.; Feng, Y.; Wang, J. Proceedings of the National Academy of Sciences, Vol. 107, Issue 31 https://doi.org/10.1073/pnas.1005036107	journal	July 2010
Integrated-fin gasket for palm cubic-anvil high pressure apparatus Cheng, J. -G.; Matsubayashi, K.; Nagasaki, S. Review of Scientific Instruments, Vol. 85, Issue 9 https://doi.org/10.1063/1.4896473	journal	September 2014
High pressure investigation of superconducting signatures in CeCu2Si2: ac-magnetic susceptibility, ac-heat capacity, resistivity and thermopower Giriat, G.; Ren, Z.; Pedrazzini, P. Solid State Communications, Vol. 209-210 https://doi.org/10.1016/j.ssc.2015.03.007	journal	May 2015
Direct probe of Fermi surface evolution across a pressure-induced quantum phase transition Feng, Yejun; Palmer, A.; Wang, Yishu Physical Review B, Vol. 91, Issue 15 https://doi.org/10.1103/PhysRevB.91.155142	journal	April 2015
A compact bellows-driven diamond anvil cell for high-pressure, low-temperature magnetic measurements Feng, Yejun; Silevitch, D. M.; Rosenbaum, T. F. Review of Scientific Instruments, Vol. 85, Issue 3 https://doi.org/10.1063/1.4867078	journal	March 2014
Heavy fermions in cerium and uranium compounds studied by the de Haas–van Alphen experiment Araki, S.; Settai, R.; Nakashima, M. Journal of Physics and Chemistry of Solids, Vol. 63, Issue 6-8 https://doi.org/10.1016/S0022-3697(02)00156-7	journal	June 2002
Critical Field and Shubnikov-de Haas Oscillations of ?-(BEDT-TTF)2Cu(NCS)2under Pressure Martin, C.; Agosta, C. C.; Tozer, S. W. Journal of Low Temperature Physics, Vol. 138, Issue 5-6 https://doi.org/10.1007/s10909-004-2898-8	journal	March 2005
New Low-Temperature Phase of Molecular Deuterium at Ultrahigh Pressure Silvera, Isaac F.; Wijngaarden, Rinke J. Physical Review Letters, Vol. 47, Issue 1 https://doi.org/10.1103/PhysRevLett.47.39	journal	July 1981
Infrared and Terahertz Spectroscopy of Strongly Correlated Electron Systems under Extreme Conditions Kimura, Shin-ichi; Okamura, Hidekazu Journal of the Physical Society of Japan, Vol. 82, Issue 2 https://doi.org/10.7566/jpsj.82.021004	journal	February 2013
Pressure-induced crystallization of a spin liquid Mirebeau, I.; Goncharenko, I. N.; Cadavez-Peres, P. Nature, Vol. 420, Issue 6911 https://doi.org/10.1038/nature01157	journal	November 2002
Pressure-Tuned Spin and Charge Ordering in an Itinerant Antiferromagnet Feng, Yejun; Jaramillo, R.; Srajer, G. Physical Review Letters, Vol. 99, Issue 13 https://doi.org/10.1103/PhysRevLett.99.137201	journal	September 2007
Pressure tuning of competing magnetic interactions in intermetallic CeFe $_{2}$ Wang, Jiyang; Feng, Yejun; Jaramillo, R. Physical Review B, Vol. 86, Issue 1 https://doi.org/10.1103/PhysRevB.86.014422	journal	July 2012
Hidden one-dimensional spin modulation in a three-dimensional metal Feng, Yejun; Wang, Jiyang; Palmer, A. Nature Communications, Vol. 5, Issue 1 https://doi.org/10.1038/ncomms5218	journal	June 2014
Metallic CsI at Pressures of up to 220 Gigapascals Eremets, M. I. Science, Vol. 281, Issue 5381 https://doi.org/10.1126/science.281.5381.1333	journal	August 1998
Recent Progress in Multi-Extreme Condition by Miniature High-Pressure Cell [高圧力発生装置の小型化による物性測定環境の拡張] Matsubayashi, Kazuyuki; Hisada, Akihiko; Kawae, Tatsuya The Review of High Pressure Science and Technology, Vol. 22, Issue 3 https://doi.org/10.4131/jshpreview.22.206	journal	January 2012
Technology of diamond anvil high-pressure cells: I. Principles, design and construction Dunstan, D. J.; Spain, I. L. Journal of Physics E: Scientific Instruments, Vol. 22, Issue 11 https://doi.org/10.1088/0022-3735/22/11/004	journal	November 1989
Cryostat for generating pressures to 100 kilobar and temperatures to 0.03 K Webb, A. W.; Gubser, D. U.; Towle, L. C. Review of Scientific Instruments, Vol. 47, Issue 1 https://doi.org/10.1063/1.1134491	journal	January 1976
Pressure calibration of diamond anvil Raman gauge to 310GPa Akahama, Yuichi; Kawamura, Haruki Journal of Applied Physics, Vol. 100, Issue 4 https://doi.org/10.1063/1.2335683	journal	August 2006
Ruby under pressure Syassen, K. High Pressure Research, Vol. 28, Issue 2 https://doi.org/10.1080/08957950802235640	journal	June 2008
Invited Article: High-pressure techniques for condensed matter physics at low temperature Feng, Yejun; Jaramillo, R.; Wang, Jiyang Review of Scientific Instruments, Vol. 81, Issue 4 https://doi.org/10.1063/1.3400212	journal	April 2010
Four-probe electrical measurements with a liquid pressure medium in a diamond anvil cell Jaramillo, R.; Feng, Yejun; Rosenbaum, T. F. Review of Scientific Instruments, Vol. 83, Issue 10 https://doi.org/10.1063/1.4757178	journal	October 2012
Simple Apparatus for Applying Uniaxial Pressure at Very Low Temperatures Ward, J. H. R. Review of Scientific Instruments, Vol. 36, Issue 9 https://doi.org/10.1063/1.1719911	journal	September 1965
Effects of pressure and temperature on exciton absorption and band structure of layer crystals: Molybdenum disulphide Connell, G. A. N.; Wilson, J. A.; Yoffe, A. D. Journal of Physics and Chemistry of Solids, Vol. 30, Issue 2 https://doi.org/10.1016/0022-3697(69)90310-2	journal	February 1969
The membrane diamond anvil cell: A new device for generating continuous pressure and temperature variations Letoullec, R.; Pinceaux, J. P.; Loubeyre, P. High Pressure Research, Vol. 1, Issue 1 https://doi.org/10.1080/08957958808202482	journal	October 1988
A diamond anvil cell for IR microspectroscopy Chervin, J. C.; Canny, B.; Besson, J. M. Review of Scientific Instruments, Vol. 66, Issue 3 https://doi.org/10.1063/1.1145594	journal	March 1995
The equation of state of solid helium: A pressure scale to 20 kbar for high pressure measurements at low temperature Spain, I. L.; Segall, S. Cryogenics, Vol. 11, Issue 1 https://doi.org/10.1016/0011-2275(71)90006-3	journal	February 1971
Nonmagnetic piston–cylinder pressure cell for use at 35 kbar and above Walker, I. R. Review of Scientific Instruments, Vol. 70, Issue 8 https://doi.org/10.1063/1.1149927	journal	August 1999
Superconductivity of Rhenium and Some Rhenium-Osmium Alloys at High Pressure Chu, C. W.; Smith, T. F.; Gardner, W. E. Physical Review Letters, Vol. 20, Issue 5 https://doi.org/10.1103/PhysRevLett.20.198	journal	January 1968
The development of an improved non-magnetic alloy based on the copper-beryllium system Jordan, B. A. Journal of Materials Science, Vol. 4, Issue 12 https://doi.org/10.1007/BF00549850	journal	December 1969
Iron cast in exotic role Saxena, S. S.; Littlewood, Peter B. Nature, Vol. 412, Issue 6844 https://doi.org/10.1038/35085681	journal	July 2001
Ferromagnetic Traces in Austenitic Stainless Steels at 4.2 k Pieterman, K.; Ketting, A.; Geerse, J. Ch. Le Journal de Physique Colloques, Vol. 45, Issue C1 https://doi.org/10.1051/jphyscol:19841127	journal	January 1984
Magnetic Susceptibility of Inconel Alloys 718, 625, and 600 at Cryogenic Temperatures Goldberg, Ira B.; Mitchell, Michael R.; Murphy, Allan R. Advances in Cryogenic Engineering Materials https://doi.org/10.1007/978-1-4613-9880-6_98	book	January 1990
Selection of Tokamak Toroidal Field Coil Case Structural Materials Wong, F. M. G.; Mitchell, N. A. Advances in Cryogenic Engineering Materials https://doi.org/10.1007/978-1-4757-9056-6_9	book	January 1998
Physical properties of Hastelloy ^® C-276™ at cryogenic temperatures Lu, J.; Choi, E. S.; Zhou, H. D. Journal of Applied Physics, Vol. 103, Issue 6 https://doi.org/10.1063/1.2899058	journal	March 2008
The Cr−Ni (Chromium-Nickel) system Nash, P. Bulletin of Alloy Phase Diagrams, Vol. 7, Issue 5 https://doi.org/10.1007/BF02867812	journal	October 1986
Measurement of Sensitization Behaviour in Ni-based Alloy 600 by means of Magnetic Property [磁性によるNi基600合金の鋭敏化挙動の測定] Okada, Yasutaka; Yoshikawa, Kunihiko; Yukitoshi, Teruo Journal of the Japan Institute of Metals, Vol. 45, Issue 5 https://doi.org/10.2320/jinstmet1952.45.5_496	journal	January 1981
Material properties of Ni Cr Al alloy and design of a 4 GPa class non-magnetic high-pressure cell Uwatoko, Yoshiya; Todo, Sakae; Ueda, Kazuhiro Journal of Physics: Condensed Matter, Vol. 14, Issue 44 https://doi.org/10.1088/0953-8984/14/44/469	journal	October 2002
The Precipitation and Strengthening Behavior of Ni₂(Mo,Cr) in HASTELLOY C-22HS Alloy, a Newly Developed High Molybdenum Ni-Base Superalloy Xie, X.; Zeng, Y.; Kou, L. Superalloys 2008 (Eleventh International Symposium) https://doi.org/10.7449/2008/Superalloys_2008_799_805	conference	January 2008
Exchange‐Enhanced Paramagnetism and Weak Ferromagnetism in the Ni ₃ Al and Ni ₃ Ga Phases; Giant Moment Inducement in Fe‐Doped Ni ₃ Ga de Boer, F. R.; Schinkel, C. J.; Biesterbos, J. Journal of Applied Physics, Vol. 40, Issue 3 https://doi.org/10.1063/1.1657528	journal	March 1969
Nanocrystalline Ni ₃ Al-type intermetallic phase powder from Ni-base superalloys Mukherji, D.; Müller, R.; Gilles, R. Nanotechnology, Vol. 15, Issue 5 https://doi.org/10.1088/0957-4484/15/5/042	journal	March 2004
Thermodynamic properties of superconducting iridium Gubser, D. U.; Soulen, R. J. Journal of Low Temperature Physics, Vol. 13, Issue 3-4 https://doi.org/10.1007/BF00654062	journal	November 1973
Effect of pressure on the superconducting transition temperature of iridium Wejgaard, W. Physics Letters A, Vol. 29, Issue 7 https://doi.org/10.1016/0375-9601(69)90324-7	journal	June 1969
Superconductivity in lithium below 0.4 millikelvin at ambient pressure Tuoriniemi, Juha; Juntunen-Nurmilaukas, Kirsi; Uusvuori, Johanna Nature, Vol. 447, Issue 7141 https://doi.org/10.1038/nature05820	journal	May 2007
Marginal breakdown of the Fermi-liquid state on the border of metallic ferromagnetism Smith, R. P.; Sutherland, M.; Lonzarich, G. G. Nature, Vol. 455, Issue 7217 https://doi.org/10.1038/nature07401	journal	October 2008
Pressure as a parameter in the study of dilute magnetic alloys Schilling, James S. Advances in Physics, Vol. 28, Issue 5 https://doi.org/10.1080/00018737900101435	journal	October 1979
Diamond anvil cell, 50th birthday Bassett, William A. High Pressure Research, Vol. 29, Issue 2 https://doi.org/10.1080/08957950802597239	journal	May 2009
Electrical resistivity measurements on fragile organic single crystals in the diamond anvil cell Adachi, T.; Tanaka, H.; Kobayashi, H. Review of Scientific Instruments, Vol. 72, Issue 5 https://doi.org/10.1063/1.1361085	journal	May 2001
Electrical Resistivity of Tetramethyltetratelluronaphtalene Crystal at Very High Pressures Examination of the Condition of Metallization of π Molecular Crystal Cui, HengBo; Okano, Yoshinori; Zhou, Biao Journal of the American Chemical Society, Vol. 130, Issue 12 https://doi.org/10.1021/ja7114025	journal	March 2008
The metal-nonmetal transition Mott, N. F.; Zinamon, Z. Reports on Progress in Physics, Vol. 33, Issue 3 https://doi.org/10.1088/0034-4885/33/3/302	journal	September 1970
Metal-insulator transition in NiS ₂ Wilson, J. A.; Pitt, G. D. The Philosophical Magazine: A Journal of Theoretical Experimental and Applied Physics, Vol. 23, Issue 186 https://doi.org/10.1080/14786437108217003	journal	June 1971
Electrical properties of $Ni S_{2 - x} {Se}_{x}$ single crystals: From Mott insulator to paramagnetic metal Yao, X.; Honig, J. M.; Hogan, T. Physical Review B, Vol. 54, Issue 24 https://doi.org/10.1103/PhysRevB.54.17469	journal	December 1996
Hydrostatic limits of 11 pressure transmitting media Klotz, S.; Chervin, J-C.; Munsch, P. Journal of Physics D: Applied Physics, Vol. 42, Issue 7, Article No. 075413 https://doi.org/10.1088/0022-3727/42/7/075413	journal	March 2009
Magnetism, structure, and charge correlation at a pressure-induced Mott-Hubbard insulator-metal transition Feng, Yejun; Jaramillo, R.; Banerjee, A. Physical Review B, Vol. 83, Issue 3 https://doi.org/10.1103/PhysRevB.83.035106	journal	January 2011

Cited By (2)

Ni–Cr–Al Alloy for neutron scattering at high pressures Cheng, Yao; Brenk, Janik; Friedrich, Bernd Materials Science and Technology, Vol. 36, Issue 9 https://doi.org/10.1080/02670836.2019.1578077	journal	February 2019
X-ray magnetic diffraction under high pressure Wang, Yishu; Rosenbaum, T. F.; Feng, Yejun IUCrJ, Vol. 6, Issue 4 https://doi.org/10.1107/s2052252519007061	journal	June 2019

Similar Records

Sub-Kelvin magnetic and electrical measurements in a diamond anvil cell with in situ tunability

Journal Article · Tue Sep 01 00:00:00 EDT 2015 · Review of Scientific Instruments · OSTI ID:1224169

Palmer, A; Silevitch, D M; Feng, Yejun; +5 more

Experimental Investigation of Magnetic Superconducting, and other Phase Transitions in Novel f-Electron Materials at Ultra-high Pressures Using Designer Diamond Anvils

Technical Report · Tue Sep 13 00:00:00 EDT 2005 · OSTI ID:1224169

Maple, M Brian

A compact bellows-driven diamond anvil cell for high-pressure, low-temperature magnetic measurements

Journal Article · Sat Mar 15 00:00:00 EDT 2014 · Review of Scientific Instruments · OSTI ID:1224169

Feng, Yejun; Silevitch, D. M.; Rosenbaum, T. F.

Related Subjects

47 OTHER INSTRUMENTATION
36 MATERIALS SCIENCE
High Pressure
Diamond Anvil Cell
Low temperature

Title: Sub-Kelvin magnetic and electrical measurements in a diamond anvil cell with in-situ tunability

Citation Formats

References (57)

Cited By (2)

Similar Records

Related Subjects