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Title: TiN coated aluminum electrodes for DC high voltage electron guns

Journal Article · · Journal of Vacuum Science and Technology A
DOI:https://doi.org/10.1116/1.4916574· OSTI ID:1190823
 [1];  [1];  [2];  [3];  [3]
  1. Old Dominion Univ., Norfolk, VA (United States)
  2. Loyola Marymount, Los Angeles, CA (United States)
  3. Thomas Jefferson National Accelerator Facility (TJNAF), Newport News, VA (United States)

Preparing electrodes made of metals like stainless steel, for use inside DC high voltage electron guns, is a labor-intensive and time-consuming process. In this paper, the authors report the exceptional high voltage performance of aluminum electrodes coated with hard titanium nitride (TiN). The aluminum electrodes were comparatively easy to manufacture and required only hours of mechanical polishing using silicon carbide paper, prior to coating with TiN by a commercial vendor. The high voltage performance of three TiN-coated aluminum electrodes, before and after gas conditioning with helium, was compared to that of bare aluminum electrodes, and electrodes manufactured from titanium alloy (Ti-6AI-4V). Following gas conditioning, each TiN-coated aluminum electrode reached -225 kV bias voltage while generating less than 100 pA of field emission (<10 pA) using a 40 mm cathode/anode gap, corresponding to field strength of 13.7 MV/m. Smaller gaps were studied to evaluate electrode performance at higher field strength with the best performing TiN-coated aluminum electrode reaching ~22.5 MV/m with field emission less than 100 pA. These results were comparable to those obtained from our best-performing electrodes manufactured from stainless steel, titanium alloy and niobium, as reported in references cited below. The TiN coating provided a very smooth surface and with mechanical properties of the coating (hardness and modulus) superior to those of stainless steel, titanium-alloy, and niobium electrodes. These features likely contributed to the improved high voltage performance of the TiN-coated aluminum electrodes.

Research Organization:
Thomas Jefferson National Accelerator Facility (TJNAF), Newport News, VA (United States)
Sponsoring Organization:
USDOE Office of Science (SC)
Grant/Contract Number:
AC05-06OR23177
OSTI ID:
1190823
Report Number(s):
JLAB-ACC-15-2090; DOE/OR/23177-3439; JVTAD6
Journal Information:
Journal of Vacuum Science and Technology A, Vol. 33, Issue 3; ISSN 0734-2101
Publisher:
American Vacuum SocietyCopyright Statement
Country of Publication:
United States
Language:
English
Citation Metrics:
Cited by: 4 works
Citation information provided by
Web of Science

References (11)

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Initiation of electrical breakdown in vacuum journal April 1973
The work function of the elements and its periodicity journal November 1977
Beneficial effects of yttrium on mechanical failure and chemical stability of the passive film in 6061 aluminum alloy journal March 2010
Variable work function in MOS capacitors utilizing nitrogen-controlled TiNx gate electrodes journal November 2004
Electrical Properties of Titanium Nitride Thin Films Deposited by Reactive Sputtering journal January 1981
Design, conditioning, and performance of a high voltage, high brightness dc photoelectron gun with variable gap journal September 2014
Improving the performance of stainless-steel DC high voltage photoelectron gun cathode electrodes via gas conditioning with helium or krypton
  • BastaniNejad, M.; Elmustafa, A. A.; Forman, E.
  • Nuclear Instruments and Methods in Physics Research Section A: Accelerators, Spectrometers, Detectors and Associated Equipment, Vol. 762 https://doi.org/10.1016/j.nima.2014.05.114
journal October 2014
Measurement of hardness and elastic modulus by instrumented indentation: Advances in understanding and refinements to methodology journal January 2004
Continuous Stiffness Measurement During Instrumented Indentation Testing journal January 2010
The correlation between the electron work function and yield strength of metals journal April 2012

Cited By (2)

Electrostatic deflector studies using small-scale prototype electrodes journal April 2019
Electrostatic deflector studies using small prototypes text January 2018

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