High rate and stable cycling of lithium metal anode

Qian, Jiangfeng; Henderson, Wesley A.; Xu, Wu; Bhattacharya, Priyanka; Engelhard, Mark H.; Borodin, Oleg; Zhang, Jiguang

doi:10.1038/ncomms7362

Title: High rate and stable cycling of lithium metal anode

Journal Article · Fri Feb 20 00:00:00 EST 2015 · Nature Communications

DOI:https://doi.org/10.1038/ncomms7362· OSTI ID:1184948

Qian, Jiangfeng ^[1]; Henderson, Wesley A. ^[1]; Xu, Wu ^[1]; Bhattacharya, Priyanka ^[2]; Engelhard, Mark H. ^[3]; Borodin, Oleg ^[4]; Zhang, Jiguang ^[1]

Pacific Northwest National Lab. (PNNL), Richland, WA (United States). Joint Center for Energy Storage Research; Pacific Northwest National Lab. (PNNL), Richland, WA (United States). Energy & Environment Directorate
Pacific Northwest National Lab. (PNNL), Richland, WA (United States). Energy & Environment Directorate
Pacific Northwest National Lab. (PNNL), Richland, WA (United States). Environmental Molecular Sciences Lab. (EMSL)
U.S. Army Research Lab., Adelphi, MD (United States). Sensor & Electron Devices Directorate

Lithium (Li) metal is an ideal anode material for rechargeable batteries. However, dendritic Li growth and limited Coulombic efficiency (CE) during repeated Li deposition/stripping processes have prevented the application of this anode in rechargeable Li metal batteries, especially for use at high current densities. Here, we report that the use of highly concentrated electrolytes composed of ether solvents and the lithium bis(fluorosulfonyl)imide (LiFSI) salt enables the high rate cycling of a Li metal anode at high CE (up to 99.1 %) without dendrite growth. With 4 M LiFSI in 1,2-dimethoxyethane (DME) as the electrolyte, a Li|Li cell can be cycled at high rates (10 mA cm^-2) for more than 6000 cycles with no increase in the cell impedance, and a Cu|Li cell can be cycled at 4 mA cm-2 for more than 1000 cycles with an average CE of 98.4%. These excellent high rate performances can be attributed to the increased solvent coordination and increased availability of Li+ concentration in the electrolyte. Lastly, further development of this electrolyte may lead to practical applications for Li metal anode in rechargeable batteries. The fundamental mechanisms behind the high rate ion exchange and stability of the electrolytes also shine light on the stability of other electrochemical systems.

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Research Organization:: Pacific Northwest National Laboratory (PNNL), Richland, WA (United States). Environmental Molecular Sciences Laboratory (EMSL)

Sponsoring Organization:: USDOE Office of Science (SC), Basic Energy Sciences (BES)

Grant/Contract Number:: AC05-76RL01830

OSTI ID:: 1184948

Report Number(s):: PNNL-SA-107989; 48379; 48316; KC0208010

Journal Information:: Nature Communications, Vol. 6; ISSN 2041-1723

Publisher:: Nature Publishing GroupCopyright Statement

Country of Publication:: United States

Language:: English

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Cited by: 1583 works

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Integrative preparation of mesoporous epoxy resin–ceramic composite electrolytes with multilayer structure for dendrite-free lithium metal batteries Li, Mengjie; Li, Hao; Lan, Jin-Le Journal of Materials Chemistry A, Vol. 6, Issue 39 https://doi.org/10.1039/c8ta06341a	journal	January 2018
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