Process for preparing a deuterated or tritiated compound

Bergman, Robert C.; Klei, Steven R.

Title: Process for preparing a deuterated or tritiated compound

Patent · Tue Sep 21 00:00:00 EDT 2004

OSTI ID:1175050

Bergman, Robert C.; Klei, Steven R.

A process for labeling organic compounds with deuterium and tritium is described using specific catalysts.

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Research Organization:: Univ. of California, Oakland, CA (United States)

Sponsoring Organization:: USDOE

DOE Contract Number:: AC03-76F00098

Assignee:: University Of California, The Regents Of

Patent Number(s):: 6,794,522

Application Number:: 10/103,481

OSTI ID:: 1175050

Country of Publication:: United States

Language:: English

References (7)

Direct tritium labeling of multifunctional compounds using organoiridium catalysis. 2. Shu, A. Y. L.; Saunders, D.; Levinson, S. H. Journal of Labelled Compounds and Radiopharmaceuticals, Vol. 42, Issue 8, p. 797-807 https://doi.org/10.1002/(SICI)1099-1344(199908)42:8<797::AID-JLCR240>3.0.CO;2-O	journal	August 1999
ChemInform Abstract: CATALYSIS BY RUTHENIUM AND RHODIUM TRIPHENYLPHOSPHINE COMPLEXES OF THE EXCHANGE OF DEUTERIUM IN THE OXYGEN-DEUTERIUM GROUP OF OCTADEUTERO-2-PROPANOL IN WATER Krutii, V. N.; Sharf, V. Z.; Yakovlev, I. P. Chemischer Informationsdienst, Vol. 7, Issue 31 https://doi.org/10.1002/chin.197631081	journal	August 1976
Deuteration of acetanilides and other substituted aromatics using [Ir(COD)(Cy3P)(Py)]PF6 as catalyst Hesk, D.; Das, P. R.; Evans, B. Journal of Labelled Compounds and Radiopharmaceuticals, Vol. 36, Issue 5 https://doi.org/10.1002/jlcr.2580360514	journal	May 1995
Monomeric (pentamethylcyclopentadienyl)iridium imido compounds: synthesis, structure, and reactivity Glueck, David S.; Wu, Jianxin; Hollander, Frederick J. Journal of the American Chemical Society, Vol. 113, Issue 6 https://doi.org/10.1021/ja00006a026	journal	March 1991
Synthesis, characterization, and reaction chemistry of new trifluoromethanesulfonato complexes of rhodium and iridium: formation of cationic rhodium-platinum and iridium-platinum heterobinuclear complexes with bridging chloride ligands Stang, Peter J.; Huang, Yo Hsin; Arif, Atta M. Organometallics, Vol. 11, Issue 1 https://doi.org/10.1021/om00037a043	journal	January 1992
Deuterium exchange labelling of substituted aromatics using [IrH2(Me2CO)2(PPh3)2]BF4 Heys, J. R.; Shu, A. Y. L.; Senderoff, S. G. Journal of Labelled Compounds and Radiopharmaceuticals, Vol. 33, Issue 5 https://doi.org/10.1002/jlcr.2580330509	journal	May 1993
Synthesis and Characterization of Hydrotris(pyrazolyl)borate Dihydrogen/Hydride Complexes of Rhodium and Iridium Oldham, Warren J.; Hinkle, Amber S.; Heinekey, D. M. Journal of the American Chemical Society, Vol. 119, Issue 45 https://doi.org/10.1021/ja971627t	journal	November 1997

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