Liquid composition having ammonia borane and decomposing to form hydrogen and liquid reaction product

Davis, Benjamin L; Rekken, Brian D

Title: Liquid composition having ammonia borane and decomposing to form hydrogen and liquid reaction product

Patent · Tue Apr 01 00:00:00 EDT 2014

OSTI ID:1129065

Davis, Benjamin L; Rekken, Brian D

Liquid compositions of ammonia borane and a suitably chosen amine borane material were prepared and subjected to conditions suitable for their thermal decomposition in a closed system that resulted in hydrogen and a liquid reaction product.

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Research Organization:: Los Alamos National Laboratory (LANL), Los Alamos, NM (United States)

Sponsoring Organization:: USDOE

DOE Contract Number:: AC52-06NA25396

Assignee:: Los Alamos National Security, LLC (Los Alamos, NM)

Patent Number(s):: 8,685,364

Application Number:: 13/850,959

OSTI ID:: 1129065

Resource Relation:: Patent File Date: 2013 Mar 26

Country of Publication:: United States

Language:: English

References (10)

Ammonia Borane Hydrogen Release in Ionic Liquids Himmelberger, Daniel W.; Alden, Laif R.; Bluhm, Martin E. Inorganic Chemistry, Vol. 48, Issue 20, p. 9883-9889 https://doi.org/10.1021/ic901560h	journal	October 2009
Amineborane-Based Chemical Hydrogen Storage: Enhanced Ammonia Borane Dehydrogenation in Ionic Liquids Bluhm, Martin E.; Bradley, Mark G.; Butterick, Robert Journal of the American Chemical Society, Vol. 128, Issue 24 https://doi.org/10.1021/ja062085v	journal	June 2006
Iridium-Catalyzed Dehydrogenation of Substituted Amine Boranes: Kinetics, Thermodynamics, and Implications for Hydrogen Storage Dietrich, Brandon L.; Goldberg, Karen I.; Heinekey, D. Michael Inorganic Chemistry, Vol. 47, Issue 19, p. 8583-8585 https://doi.org/10.1021/ic801161g	journal	October 2008
Syntheses and Structural Characterizations of Anionic Borane-Capped Ammonia Borane Oligomers: Evidence for Ammonia Borane H ₂ Release via a Base-Promoted Anionic Dehydropolymerization Mechanism Ewing, William C.; Marchione, Allegra; Himmelberger, Daniel W. Journal of the American Chemical Society, Vol. 133, Issue 42 https://doi.org/10.1021/ja207971h	journal	October 2011
Efficient synthesis and NMR data of N- or B-substituted borazines Framery, Eric; Vaultier, Michel Heteroatom Chemistry, Vol. 11, Issue 3, p. 218-225 https://doi.org/10.1002/(SICI)1098-1071(2000)11:3<218::AID-HC10>3.0.CO;2-K	journal	January 2000
Thermochemistry for the Dehydrogenation of Methyl-Substituted Ammonia Borane Compounds Grant, Daniel J.; Matus, Myrna H.; Anderson, Kevin D. The Journal of Physical Chemistry A, Vol. 113, Issue 21 https://doi.org/10.1021/jp902196d	journal	May 2009
B–N compounds for chemical hydrogenstorage Hamilton, Charles W.; Baker, R. Tom; Staubitz, Anne Chem. Soc. Rev., Vol. 38, Issue 1, p. 279-293 https://doi.org/10.1039/B800312M	journal	January 2009
Transition metal catalysed dehydrogenation of amine-borane fuel blends Mal, Sib Sankar; Stephens, Frances H.; Baker, R. Tom Chemical Communications, Vol. 47, Issue 10 https://doi.org/10.1039/C0CC03585H	journal	January 2011
Ammonia-Borane and Related Compounds as Dihydrogen Sources Staubitz, Anne; Robertson, Alasdair P. M.; Manners, Ian Chemical Reviews, Vol. 110, Issue 7 https://doi.org/10.1021/cr100088b	journal	July 2010
Iridium-Catalyzed Dehydrocoupling of Primary Amine-Borane Adducts: A Route to High Molecular Weight Polyaminoboranes, Boron-Nitrogen Analogues of Polyolefins Staubitz, Anne; Presa Soto, Alejandro; Manners, Ian Angewandte Chemie, Vol. 120, Issue 33, p. 6308-6311 https://doi.org/10.1002/ange.200801197	journal	August 2008

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