Method for fabricating apatite crystals and ceramics

Soules, Thomas F.; Schaffers, Kathleen I.; Tassano, Jr., John B.; Hollingsworth, Joel P.

Title: Method for fabricating apatite crystals and ceramics

Patent · Tue Sep 10 00:00:00 EDT 2013

OSTI ID:1092934

Soules, Thomas F.; Schaffers, Kathleen I.; Tassano, Jr., John B.; Hollingsworth, Joel P.

The present invention provides a method of crystallizing Yb:C-FAP [Yb.sup.3+:Ca.sub.5(PO.sub.4).sub.3F], by dissolving the Yb:C-FAP in an acidic solution, following by neutralizing the solution. The present invention also provides a method of forming crystalline Yb:C-FAP by dissolving the component ingredients in an acidic solution, followed by forming a supersaturated solution.

View Patent

Cite

Export

Save

Research Organization:: Lawrence Livermore National Laboratory (LLNL), Livermore, CA (United States)

Sponsoring Organization:: USDOE

DOE Contract Number:: AC52-07NA27344

Assignee:: Lawrence Livermore National Security, LLC (Livermore, CA)

Patent Number(s):: 8,529,859

Application Number:: 13/043,072

OSTI ID:: 1092934

Country of Publication:: United States

Language:: English

References (15)

Molecular modulation of calcium oxalate crystallization De Yoreo, James J.; Qiu, S. Roger; Hoyer, John R. American Journal of Physiology-Renal Physiology, Vol. 291, Issue 6 https://doi.org/10.1152/ajprenal.00136.2006	journal	December 2006
Comb-drive micromechanical tuning fork gyroscope with piezoelectric readout Bernstein, Jonathan J.; Weinberg, Marc S. https://doi.org/https://image-ppubs.uspto.gov/dirsearch-public/print/downloadPdf/5767405 US Patent Document 5,767,405	patent	June 1998
Controlled Crystallization of Calcium Phosphate Apatites Rodríguez-Lorenzo, L. M.; Vallet-Regí, M. Chemistry of Materials, Vol. 12, Issue 8 https://doi.org/10.1021/cm001033g	journal	August 2000
Influence of nickel on hydroxyapatite crystallization: Influence of Ni on hydroxyapatite crystallization Guerra-López, J.; Pomés, R.; Védova, C. O. Della Journal of Raman Spectroscopy, Vol. 32, Issue 4 https://doi.org/10.1002/jrs.689	journal	April 2001
Growth of Yb: S-FAP [Yb3+:Sr5(PO4)3F] crystals for the Mercury laser Schaffers, K. I.; Tassano, J. B.; Bayramian, A. B. Journal of Crystal Growth, Vol. 253, Issue 1-4 https://doi.org/10.1016/S0022-0248(03)01032-7	journal	June 2003
Chitosan membrane as a template for hydroxyapatite crystal growth in a model dual membrane diffusion system Ehrlich, H.; Krajewska, B.; Hanke, T. Journal of Membrane Science, Vol. 273, Issue 1-2 https://doi.org/10.1016/j.memsci.2005.11.050	journal	March 2006
Calcium hydroxyapatite ceramic implants in bone tumour surgery: A LONG-TERM FOLLOW-UP STUDY Matsumine, A.; Myoui, A.; Kusuzaki, K. The Journal of Bone and Joint Surgery. British volume, Vol. 86-B, Issue 5 https://doi.org/10.1302/0301-620X.86B5.14242	journal	July 2004
Simultaneous crystallization of calcium phosphate and calcium oxalate in the presence of ascorbic acid under physiological conditions Vani, R.; Girija, E. K.; Palanichamy, M. Materials Science and Engineering: C, Vol. 29, Issue 4 https://doi.org/10.1016/j.msec.2008.09.030	journal	May 2009
Crystal growth, spectroscopic characterization, and laser performance of a new efficient laser material Nd:Ba5(PO4)3F Loutts, G. B.; Bonner, C.; Meegoda, C. Applied Physics Letters, Vol. 71, Issue 3 https://doi.org/10.1063/1.119556	journal	July 1997
Laser, optical, and thermomechanical properties of Yb-doped fluorapatite Payne, S. A.; Smith, L. K.; DeLoach, L. D. IEEE Journal of Quantum Electronics, Vol. 30, Issue 1 https://doi.org/10.1109/3.272077	journal	January 1994
The nucleation and growth of calcium phosphate by amelogenin Tarasevich, Barbara J.; Howard, Christopher J.; Larson, Jenna L. Journal of Crystal Growth, Vol. 304, Issue 2 https://doi.org/10.1016/j.jcrysgro.2007.02.035	journal	June 2007
Growth of high-quality single crystals of FAP (Ca5(PO4)3F) and its isomorphs Loutts, G. B.; Chai, Bruce H. T. OE/LASE'93: Optics, Electro-Optics, & Laser Applications in Science& Engineering, SPIE Proceedings https://doi.org/10.1117/12.149284	conference	July 1993
Preparation and characterization of calcium hydroxyapatite and balloon-like calcium phosphate particles from forced hydrolysis of Ca(OH)2–triphosphate solution Kandori, Kazuhiko; Takeguchi, Kazuma; Fukusumi, Masao Polyhedron, Vol. 28, Issue 14 https://doi.org/10.1016/j.poly.2009.06.023	journal	September 2009
Inhibition of calcium phosphate crystallization by nucleoside phosphates Meyer, John L.; McCall, John T.; Smith, Lynwood H. Calcified Tissue Research, Vol. 15, Issue 1 https://doi.org/10.1007/BF02059063	journal	December 1974
Rapid growth of KDP-type crystals Zaitseva, N.; Carman, L. Progress in Crystal Growth and Characterization of Materials, Vol. 43, Issue 1 https://doi.org/10.1016/S0960-8974(01)00004-3	journal	January 2001

Similar Records

Hybrid solid state laser system using a neodymium-based master oscillator and an ytterbium-based power amplifier

Patent · Mon Jan 01 00:00:00 EST 2001 · OSTI ID:1092934

Payne, Stephen A; Marshall, Christopher D; Powell, Howard T; +1 more

Ceramic materials with low thermal conductivity and low coefficients of thermal expansion

Patent · Wed Jan 01 00:00:00 EST 1992 · OSTI ID:1092934

Brown, Jesse; Hirschfeld, Deidre; Liu, Dean-Mo; +5 more

Influences on Subsurface Plutonium and Americium Migration

Journal Article · Thu Feb 04 00:00:00 EST 2021 · ACS Earth and Space Chemistry · OSTI ID:1092934

Emerson, Hilary P.; Pearce, Carolyn I.; Delegard, Calvin H.; +15 more

Related Subjects

37 INORGANIC, ORGANIC, PHYSICAL, AND ANALYTICAL CHEMISTRY

Title: Method for fabricating apatite crystals and ceramics

Citation Formats

References (15)

Similar Records

Related Subjects