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Title: Development of an advanced continuous mild gasification process for the production of coproducts. Task 4, System integration studies: Char upgrading

Technical Report ·
DOI:https://doi.org/10.2172/10145427· OSTI ID:10145427

This document describes the results of Task 4 under which a 50 pound/hour char-to-carbon (CTC) process research unit (PRU) was designed in the second half of 1989, with construction completed in June 1990. The CTC PRU at Golden was operated for nearly one year during which 35 runs were completed for a total of nearly 800 hours of operation. Char methanation and carbon production reactor development activities are detailed in this report, as well as the results of integrated runs of the CTC process. Evaluation of the process and the carbon product produced is also included. It was concluded that carbon could be produced from mild gasification char utilizing the CTC process. Char methanation and membrane separation steps performed reasonably well and can scaled up with confidence. However, the novel directly heated reactor system for methane cracking did not work satisfactorily due to materials of construction and heat transfer problems, which adversely affected the quantity and quality of the carbon product. Alternative reactor designs are recommended.

Research Organization:
Western Research Inst., Laramie, WY (United States); AMAX Research and Development Center, Golden, CO (United States)
Sponsoring Organization:
USDOE, Washington, DC (United States)
DOE Contract Number:
AC21-87MC24268
OSTI ID:
10145427
Report Number(s):
DOE/MC/24268-3076; ON: DE92001262
Resource Relation:
Other Information: PBD: Dec 1991
Country of Publication:
United States
Language:
English