X-ray study of interfacial interactions in highly milled Sn-Ge powders
Abstract
We have studied possible structural changes occurring at the Sn/Ge interface of highly milled Sn/Ge composites. EXAFS and X-ray Diffraction measurements were made on mechanically milled powders having compositions ranging from 20 to 50 vol.% Sn. X-ray diffraction measurements indicate the increasing amorphization of Sn as the Sn content is decreased. EXAFS results indicate that this amorphous phase is due to the formation of an {alpha}-Sn/Ge alloy. The EXAFS from this alloy did not change significantly at the Sn melting point. X-ray diffraction measurements made at room temperature show a systematic decrease in the intensity of Sn peaks and broadening of Ge peaks with the decreasing Sn content.
- Authors:
- Publication Date:
- Research Org.:
- Brookhaven National Lab., Upton, NY (United States)
- Sponsoring Org.:
- USDOE, Washington, DC (United States)
- OSTI Identifier:
- 10143610
- Report Number(s):
- BNL-47382; CONF-911202-78
ON: DE92012518
- DOE Contract Number:
- AC02-76CH00016; AS05-80ER10742
- Resource Type:
- Conference
- Resource Relation:
- Conference: Annual fall meeting of the Materials Research Society (MRS),Boston, MA (United States),2-6 Dec 1991; Other Information: PBD: [1991]
- Country of Publication:
- United States
- Language:
- English
- Subject:
- 36 MATERIALS SCIENCE; TIN; INTERFACES; GERMANIUM; X-RAY DIFFRACTION; POWDERS; TEMPERATURE DEPENDENCE; MELTING POINTS; SOLUBILITY; LATTICE PARAMETERS; CHEMICAL BONDS; AMORPHOUS STATE; 360102; STRUCTURE AND PHASE STUDIES
Citation Formats
Jayanetti, J K.D.S., Heald, S M, and Tan, Z. X-ray study of interfacial interactions in highly milled Sn-Ge powders. United States: N. p., 1991.
Web.
Jayanetti, J K.D.S., Heald, S M, & Tan, Z. X-ray study of interfacial interactions in highly milled Sn-Ge powders. United States.
Jayanetti, J K.D.S., Heald, S M, and Tan, Z. 1991.
"X-ray study of interfacial interactions in highly milled Sn-Ge powders". United States. https://www.osti.gov/servlets/purl/10143610.
@article{osti_10143610,
title = {X-ray study of interfacial interactions in highly milled Sn-Ge powders},
author = {Jayanetti, J K.D.S. and Heald, S M and Tan, Z},
abstractNote = {We have studied possible structural changes occurring at the Sn/Ge interface of highly milled Sn/Ge composites. EXAFS and X-ray Diffraction measurements were made on mechanically milled powders having compositions ranging from 20 to 50 vol.% Sn. X-ray diffraction measurements indicate the increasing amorphization of Sn as the Sn content is decreased. EXAFS results indicate that this amorphous phase is due to the formation of an {alpha}-Sn/Ge alloy. The EXAFS from this alloy did not change significantly at the Sn melting point. X-ray diffraction measurements made at room temperature show a systematic decrease in the intensity of Sn peaks and broadening of Ge peaks with the decreasing Sn content.},
doi = {},
url = {https://www.osti.gov/biblio/10143610},
journal = {},
number = ,
volume = ,
place = {United States},
year = {Tue Dec 31 00:00:00 EST 1991},
month = {Tue Dec 31 00:00:00 EST 1991}
}
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