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Title: Analysis of deposit from K-Reactor heat exchanger 4A. Revision 1

Technical Report ·
DOI:https://doi.org/10.2172/10136631· OSTI ID:10136631

Characterization of deposits from the reactor system provides a means of directly assessing corrosion and chemistry conditions within the system. The recent analysis of debris vacuumed from the bottom of K-Reactor tank provided information and reassurance about the conditions within the tank that would affect corrosion or moderator chemistry. Further opportunity for surveillance within the reactor system was recognized when solid deposits were found on the moderator side of the K-Reactor heat exchanger 4A that failed in December 1991. A sample of deposited material from the face of the tube sheet at the inlet end was removed under the direction of Equipment Engineering Section personnel. The material was analyzed by the Analytical Development Section by techniques used earlier for the K-tank debris. Elemental content was determined by Scanning Electron Microscopy/Energy Dispersive Spectroscopy (SEM/EDS). Total chlorine content was determined by neutron activation analysis. Crystalline components were identified by X-Ray diffraction, and radionuclidic content characterized by alpha pulse height analysis, beta counting, scintillation counting, and gamma spectroscopy. The purpose of this memorandum is to report the results of these analyses.

Research Organization:
Savannah River Site (SRS), Aiken, SC (United States)
Sponsoring Organization:
USDOE, Washington, DC (United States)
DOE Contract Number:
AC09-89SR18035
OSTI ID:
10136631
Report Number(s):
WSRC-TR-92-139-Rev.1; ON: DE93008797
Resource Relation:
Other Information: PBD: 20 Mar 1992
Country of Publication:
United States
Language:
English