Cryogenic focussing, ohmically heated on-column trap
Conference
·
OSTI ID:10119643
A procedure is described for depositing a conductive layer of gold on the exterior of a fused-silica capillary used in gas chromatography. By subjecting a section of the column near the inlet to a thermal cycle of cryogenic cooling and ohmic heating, volatile samples are concentrated and subsequently injected. The performance of this trap as a chromatographic injector is demonstrated. Several additional applications are suggested and the unique properties of this device are discussed. 11 refs., 5 figs., 1 tab.
- Research Organization:
- Brookhaven National Lab., Upton, NY (United States)
- Sponsoring Organization:
- USDOE, Washington, DC (United States)
- DOE Contract Number:
- AC02-76CH00016
- OSTI ID:
- 10119643
- Report Number(s):
- BNL-46980; CONF-911231-5; ON: DE92007181
- Resource Relation:
- Conference: Technology 2001: 2nd national technology transfer conference and exposition,San Jose, CA (United States),3-5 Dec 1991; Other Information: PBD: Dec 1991
- Country of Publication:
- United States
- Language:
- English
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