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  1. Critical differences between electron beam melted and selective laser melted Ti-6Al-4 V

    Effective optimization of the production of Ti-6Al-4 V using AM requires a fundamental understanding of the relative importance of different microstructural features to the deformation and failure mechanisms, particularly features that vary between production methods. In this study, the tensile response and deformation mechanisms of electron beam melted (EBM) AM Ti-6Al-4 V material loaded in different orientations and produced using various powder sizes were compared to those of selective laser melted (SLM) AM Ti-6Al-4 V material. The density and morphology of pores, phase fractions, prior-β grains, and defect microstructures were evaluated using scanning electron microscopy, X-ray computed tomography, electron backscattermore » diffraction, and transmission electron microscopy before and after deformation. The results were used to evaluate the relative importance of each feature on strengthening, deformation, and failure initiation mechanisms. Results focused primarily on coarse-powder EBM materials indicated that phase distribution and defect density were most influential for determining material yield strength as well as maximum possible strain to failure. Porosity was lower overall in EBM Ti-6Al-4 V than in SLM, allowing for occasional increases in part strain to failure, but remained a limiting factor determining overall part ductility.« less
  2. Nondiffractive beam shaping for enhanced optothermal control in metal additive manufacturing

    High thermal gradients and complex melt pool instabilities involved in powder bed fusion–based metal additive manufacturing using focused Gaussian-shaped beams often lead to high porosity, poor morphological quality, and degraded mechanical performance. We show here that Bessel beams offer unprecedented control over the spatiotemporal evolution of the melt pool in stainless steel (SS 316L) in comparison to Gaussian beams. Notably, the nondiffractive nature of Bessel beams enables greater tolerance for focal plane positioning during 3D printing. We also demonstrate that Bessel beams significantly reduce the propensity for keyhole formation across a broad scan parameter space. High-speed imaging of the meltmore » pool evolution and solidification dynamics reveals a unique mechanism where Bessel beams stabilize the melt pool turbulence and increase the time for melt pool solidification, owing to reduced thermal gradients. Consequently, we observe a distinctively improved combination of high density, reduced surface roughness, and robust tensile properties in 3D-printed test structures.« less
  3. Controlling interdependent meso-nanosecond dynamics and defect generation in metal 3D printing

    State-of-the-art metal 3D printers promise to revolutionize manufacturing, yet they have not reached optimal operational reliability. The challenge is to control complex laser–powder–melt pool interdependency (dependent upon each other) dynamics. We used high-fidelity simulations, coupled with synchrotron experiments, to capture fast multitransient dynamics at the meso-nanosecond scale and discovered new spatter-induced defect formation mechanisms that depend on the scan strategy and a competition between laser shadowing and expulsion. We derived criteria to stabilize the melt pool dynamics and minimize defects. This will help improve build reliability.
  4. In situ measurements of layer roughness during laser powder bed fusion additive manufacturing using low coherence scanning interferometry

    Here, layer-to-layer height measurements of additively manufactured 316L stainless steel using high speed spectral-domain optical coherence tomography (SD-OCT) are presented. Layers are built up using an open architecture laser powder bed fusion machine while height measurements are made in-line along the process laser path following each layer print. Printed cubes, with and without an internal ‘overhang’ channel, were built to investigate the effect of scanning parameters on surface structure. Layer-to-layer scan rotation strategy significantly impacts surface roughness between layers which in turn can influence porosity. Spatter particles, which have been correlated with numerous defect modalities, generate high points in themore » powder bed and can persist on a melted surface for many layers. Laser power significantly affects overhang morphology, as measured by SD-OCT. Large dross occurs in the high energy density regime, while balling and a capillary-driven coalescence of unstable melt pools perpendicular to the scanning direction occurs in the low energy density regime. High fidelity powder-scale simulations of deep powder layers were used to further elucidate the underlying physics revealed by SD-OCT measurements and high speed imaging, yielding insight to defect formation mechanisms which can lead to improved process parameters.« less
  5. Energy Coupling Mechanisms and Scaling Behavior Associated with Laser Powder Bed Fusion Additive Manufacturing

    In situ optical absorptivity measurements are carried out to clarify the physics of the laser-material interactions involved and to validate both finite element and analytical models describing laser powder bed fusion processing. Absorption of laser energy is evaluated directly using precise calorimetry measurements and compared to melt pool depths for common structural metal alloys (Ti-6Al-4V, Inconel 625, and stainless steel 316L) as a function of incident laser power, scan velocity and laser beam diameter. Changes in both absorptivity and melt pool depths for all materials are found to vary strongly across the conduction-keyhole mode threshold. A hydrodynamic finite element modelmore » is coupled to a ray-tracing-based absorptivity model, yielding excellent agreement with the experimental results and elucidating additional physics. The experimental results are further analyzed using normalized enthalpy (β) and normalized thermal diffusion length (L*th) relations and demonstrate that the normalized melt pool depth (d* = d/a, where d is melt pool depth and a is beam radius) is proportional to βL*th, while absorptivity follows an asymptotic exponential function against βL*th. Expressions for melt pool depth and laser absorptivity across different materials and laser scan systems are derived and thus provide useful tools to accelerate the optimization of laser processing parameters for metal 3D printing processes.« less
  6. Denudation of metal powder layers in laser powder bed fusion processes

    Understanding laser interaction with metal powder beds is critical in predicting optimum processing regimes in laser powder bed fusion additive manufacturing of metals. In this work, we study the denudation of metal powders that is observed near the laser scan path as a function of laser parameters and ambient gas pressure. We show that the observed depletion of metal powder particles in the zone immediately surrounding the solidified track is due to a competition between outward metal vapor flux directed away from the laser spot and entrainment of powder particles in a shear flow of gas driven by a metalmore » vapor jet at the melt track. Between atmospheric pressure and ~10 Torr of Ar gas, the denuded zone width increases with decreasing ambient gas pressure and is dominated by entrainment from inward gas flow. The denuded zone then decreases from 10 to 2.2 Torr reaching a minimum before increasing again from 2.2 to 0.5 Torr where metal vapor flux and expansion from the melt pool dominates. In addition, the dynamics of the denudation process were captured using high-speed imaging, revealing that the particle movement is a complex interplay among melt pool geometry, metal vapor flow, and ambient gas pressure. The experimental results are rationalized through finite element simulations of the melt track formation and resulting vapor flow patterns. The results presented here represent new insights to denudation and melt track formation that can be important for the prediction and minimization of void defects and surface roughness in additively manufactured metal components.« less

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