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Title: Measuring Curved Crystal Performance for a High Resolution, Imaging X-ray Spectrometer

Journal Article · · X-Ray Optics and Instrumentation

This paper describes the design, crystal selection, and crystal testing for a vertical Johann spectrometer operating in the 13 keV range to measure ion Doppler broadening in inertial confinement plasmas. The spectrometer is designed to use thin, curved, mica crystals to achieve a resolving power of E/ΔE>2000. A number of natural mica crystals were screened for flatness and X-ray diffraction width to find samples of sufficient perfection for use in the instrument. Procedures to select and mount high quality mica samples are discussed. A diode-type X-ray source coupled to a dual goniometer arrangement was used to measure the crystal reflectivity curve. A procedure was developed for evaluating the goniometer performance using a set of diffraction grade Si crystals. This goniometer system was invaluable for identifying the best original crystals for further use and developing the techniques to select satisfactory curved crystals for the spectrometer.

Research Organization:
National Security Technologies, LLC (United States)
Sponsoring Organization:
USDOE; USDOE National Nuclear Security Administration (NA)
DOE Contract Number:
DE-AC52-06NA25946
OSTI ID:
993431
Report Number(s):
DOE/NV/25946-839; TRN: US1100007
Journal Information:
X-Ray Optics and Instrumentation, Vol. 2010
Publisher:
Hindawi Publishing Corporation
Country of Publication:
United States
Language:
English