Quantitative determination of lead in mixtures of lead(II) halidesusing solid-state 207pb nmr spectroscopy
A multi-spectrum technique for facile, quantitativedetermination of lead in solid materials using solid-state 207Pb NMR thatavoids the major problem of uniform excitation across a wide spectralrange has been demonstrated. The method can be employed without chemicalseparation or other chemical manipulations and without any prior samplepreparation, resulting in a non-destructive analysis, and producingresults that are in agreement with gravimetric analyses of mixed samplesof the lead halides.
- Research Organization:
- COLLABORATION - University ofDelaware
- DOE Contract Number:
- DE-AC02-05CH11231
- OSTI ID:
- 910242
- Report Number(s):
- LBNL-63086; TRN: US0704133
- Journal Information:
- The Analyst, Vol. 131; Related Information: Journal Publication Date: 2006
- Country of Publication:
- United States
- Language:
- English
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