EPA (Environmental Protection Agency) method study 14, Method 604-Phenols. Report for 18 Sep 78-30 Mar 84
An interlaboratory study in which 20 laboratories participated was conducted to provide precision and accuracy statements for the proposed EPA Method 604-Phenols for measuring concentrations of the Category 8 chemicals phenol, 2,4-dimethylphenol, 2-chlorophenol, 4-chloro-3-methylphenol, 2,4-dichlorophenol, 2,4,6-trichlorophenol, pentachlorophenol, 2-nitrophenol, 4-nitrophenol, 4,6-dinitro-2-methylphenol, and 2,4-dinitrophenol in municipal and industrial aqueous discharges. The method provides for the determination of the phenols by gas chromatography (GC) with flame ionization detection (FID) or derivatization and detection by electron capture (EC). The study design was based on Youden's plan for collaborative tests of analytical methods. Three Youden pair samples of the test compounds were spiked into six types of test waters and then analyzed.
- Research Organization:
- IT Enviroscience, Knoxville, TN (USA)
- OSTI ID:
- 6604961
- Report Number(s):
- PB-84-196211
- Country of Publication:
- United States
- Language:
- English
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37 INORGANIC
ORGANIC
PHYSICAL AND ANALYTICAL CHEMISTRY
PHENOLS
INTERLABORATORY COMPARISONS
QUANTITATIVE CHEMICAL ANALYSIS
GAS CHROMATOGRAPHY
INDUSTRIAL WASTES
PHENOL
SEWAGE
WATER POLLUTION
AROMATICS
CHEMICAL ANALYSIS
CHROMATOGRAPHY
HYDROXY COMPOUNDS
ORGANIC COMPOUNDS
POLLUTION
SEPARATION PROCESSES
WASTES
520200* - Environment
Aquatic- Chemicals Monitoring & Transport- (-1989)
400100 - Analytical & Separations Chemistry