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Title: Purification of caprolactam from recycled nylon

Patent ·
OSTI ID:6439874

A method is disclosed of removing 1,11-diamino-6-undecanone from the pyrolysis product of nylon comprising: (a) pyrolyzing nylon-6 to form a pyrolyzate containing a caprolactam mixture; (b) dissolving the caprolactam mixture in a solvent to form a solution; (c) passing carbon dioxide gas through the solution to form a precipitate; (d) removing the precipitate from the solution; and (e) recovering the purified caprolactam from the solution. 3 figs.

Sponsoring Organization:
USDOE; USDOE, Washington, DC (United States)
DOE Contract Number:
AC36-83CH10093
Assignee:
Midwest Research Inst., Kansas City, MO (United States)
Patent Number(s):
US 5919927; A
Application Number:
PPN: US 9-058403
OSTI ID:
6439874
Resource Relation:
Patent File Date: 9 Apr 1998
Country of Publication:
United States
Language:
English