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Title: Wilmington crude oil and addendum

Abstract

Ten (10) ampoules of the Wilmington crude oil material have been analyzed by gas chromatography/mass spectrometry (GC/MS). The measurements were made directly on samples of the diluted oil by GC/MS with selected ion monitoring (SIM). The mass spectrometer was operated in the chemical ionization mode using methane as the reagent gas, and the method of internal standards was used for the quantitative measurements. The analytes determined in the Wilmington crude oil are shown in Table 1. For most of the analytes, the quasi-molecular ion (M+H)/sup +/ was the species on which the SIM measurements were made. For measurements on the second set of ampoules, m/z 252 (M)/sup +/ was monitored for the benzo(a)pyrene, benzo(e)pyrene, and perylene. The ion(s) monitored for each of the analytes is also shown in Table 1. 4 tabs.

Publication Date:
Research Org.:
National Bureau of Standards, Washington, DC (USA)
OSTI Identifier:
6321052
Report Number(s):
DOE/ER/60043-T4
ON: DE86003525
DOE Contract Number:  
AT01-82ER60043
Resource Type:
Technical Report
Country of Publication:
United States
Language:
English
Subject:
02 PETROLEUM; PETROLEUM; GAS CHROMATOGRAPHY; MASS SPECTROSCOPY; BENZOPYRENE; CARBAZOLES; CHEMICAL ANALYSIS; CONDENSED AROMATICS; EXPERIMENTAL DATA; PERYLENE; PHENANTHRENE; PYRENE; US NBS; AROMATICS; AZAARENES; AZOLES; CHROMATOGRAPHY; DATA; ENERGY SOURCES; FOSSIL FUELS; FUELS; HETEROCYCLIC COMPOUNDS; HYDROCARBONS; INFORMATION; NATIONAL ORGANIZATIONS; NUMERICAL DATA; ORGANIC COMPOUNDS; ORGANIC NITROGEN COMPOUNDS; SEPARATION PROCESSES; SPECTROSCOPY; US DOC; US ORGANIZATIONS; 023000* - Petroleum- Properties & Composition

Citation Formats

. Wilmington crude oil and addendum. United States: N. p., 1983. Web.
. Wilmington crude oil and addendum. United States.
. 1983. "Wilmington crude oil and addendum". United States.
@article{osti_6321052,
title = {Wilmington crude oil and addendum},
author = {},
abstractNote = {Ten (10) ampoules of the Wilmington crude oil material have been analyzed by gas chromatography/mass spectrometry (GC/MS). The measurements were made directly on samples of the diluted oil by GC/MS with selected ion monitoring (SIM). The mass spectrometer was operated in the chemical ionization mode using methane as the reagent gas, and the method of internal standards was used for the quantitative measurements. The analytes determined in the Wilmington crude oil are shown in Table 1. For most of the analytes, the quasi-molecular ion (M+H)/sup +/ was the species on which the SIM measurements were made. For measurements on the second set of ampoules, m/z 252 (M)/sup +/ was monitored for the benzo(a)pyrene, benzo(e)pyrene, and perylene. The ion(s) monitored for each of the analytes is also shown in Table 1. 4 tabs.},
doi = {},
url = {https://www.osti.gov/biblio/6321052}, journal = {},
number = ,
volume = ,
place = {United States},
year = {Tue Mar 29 00:00:00 EST 1983},
month = {Tue Mar 29 00:00:00 EST 1983}
}

Technical Report:
Other availability
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