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Title: Data analysis methods for flash thermal diffusivity experiments

Technical Report ·
DOI:https://doi.org/10.2172/6312039· OSTI ID:6312039

New methods, based on nonlinear least squares techniques, are presented for reducing flash diffusivity data obtained on layered composite samples. Analytical solutions to the transient heat conduction equation are derived by the Laplace transform technique for the cases of two and three layer samples with interfacial thermal resistance between the layers and thermal losses at the external boundaries. The use of the analytical solutions in least squares fitting programs is then discussed, with emphasis on the two layer problem. A description of FORTRAN computer programs which implement the calculations is given, with emphasis on the non-linear least squares fitting routine LSTSQRSL3. This program can determine the external boundary thermal loss factor and either the thermal diffusivity of one of the layers or the interfacial resistance between the layers. Two examples of the use of this program are given. In the first, the thermal diffusivity of an alumina layer in a graphite-alumina sample is determined, and in the second, the diffusivity of an enamel paint on a stainless steel substrate is determined. 34 refs., 12 figs., 2 tabs.

Research Organization:
Sandia National Lab. (SNL-NM), Albuquerque, NM (United States)
DOE Contract Number:
AC04-76DP00789
OSTI ID:
6312039
Report Number(s):
SAND-89-0260; ON: DE89010274
Resource Relation:
Other Information: Portions of this document are illegible in microfiche products
Country of Publication:
United States
Language:
English