Small-angle x-ray scattering investigation of the effect of heating temperature on the submicroscopic pore structure of wood charcoal
In order to learn about the effects of higher preparation temperatures, we recently examined a series of charcoals from black cherry (Prunus serotina Ehrh.) wood heated to temperatures from 600/sup 0/ to 2000/sup 0/C. The results are summarized in this report. In addition to obtaining some information about the pore structure of black cherry charcoal, we have developed a general picture of how the charcoal porosity depends on the temperature to which the wood was heated during pyrolysis. These results have led us to propose that the macropores in charcoals are similar to those in wood and that the main effect which pyrolysis at temperatures above 400/sup 0/C exerts on the pore structure is to cause the micropores and transitional pores to grow, while leaving the macropores almost unchanged.
- Research Organization:
- Physics Department, University of Missouri, Columbia, MO
- OSTI ID:
- 6082196
- Journal Information:
- Prepr. Pap., Am. Chem. Soc., Div. Fuel Chem.; (United States), Vol. 29:2
- Country of Publication:
- United States
- Language:
- English
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Related Subjects
ORGANIC
PHYSICAL AND ANALYTICAL CHEMISTRY
CHARCOAL
PYROLYSIS
X-RAY DIFFRACTION
HIGH TEMPERATURE
MICROSTRUCTURE
POROSITY
TEMPERATURE EFFECTS
WOOD FUELS
ADSORBENTS
CHEMICAL REACTIONS
COHERENT SCATTERING
CRYSTAL STRUCTURE
DECOMPOSITION
DIFFRACTION
ENERGY SOURCES
FUELS
SCATTERING
THERMOCHEMICAL PROCESSES
400800* - Combustion
Pyrolysis
& High-Temperature Chemistry