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Title: Recovery of fine coal from waste streams using advanced column flotation

Technical Report ·
OSTI ID:5925497

The overall objective of this program is to evaluate the application of an advanced physical separation technique, namely Ken-Flote column flotation to maximize BTU recovery with minimum product sulfur and ash content from two Illinois coal preparation plant fine waste streams. The project will optimize various operating parameters with particular emphasis on fine bubble generating devices and reagent packages to enhance the rejection of liberated ash and pyrite. During this contract period, samples were obtained from the Kerr-McGee Galatia Preparation Plant and characterized. Analysis of the flotation feed slurry indicate that a significant amount of pyrite is present in the 5 microns size range as free particles. The coal is hydrophobic in nature and optimum reagent addition is 0.75 lb/ton frother and 1.5 lb/ton fuel oil. The best flotation results were obtained near pH 6 for all frothers tested. Two ash depressants tested showed no significant improvement in ash rejection. A pyrite depressant was also tested which indicated improved pyrite rejection from 28 to 37 percent at a dosage of 5 lb/ton. Efforts are in progress to design a test matrix to determine optimum operating conditions for column flotation testing with this substrate. The test matrixes will be designed to investigate three different bubble generating mechanisms. The objective is to identify column operating variables that will provide maximum combustible recovery, minimum product ash and maximum pyrite rejection. 10 figs., 1 tab.

Research Organization:
Kentucky Univ., Lexington, KY (USA). Center for Applied Energy Research
Sponsoring Organization:
USDOE; USDOE, Washington, DC (USA)
DOE Contract Number:
FG22-90PC90176
OSTI ID:
5925497
Report Number(s):
DOE/PC/90176-T4; ON: DE91010503
Country of Publication:
United States
Language:
English