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Title: Fabrication, phase transformation studies and characterization of SiC-AlN-Al sub 2 OC ceramics

Technical Report ·
OSTI ID:5554507

The principal objective of the work has been to examine phase relations, phase transformations, the resulting precipitate morphologies and their influence on high temperature creep of the SiC-A1N-Al{sub 2}OC ceramics. This system was chosen as prior work has shown the existence of extensive of solid solubility at elevated temperatures and tendency for phase separation at lower temperatures. Phase separation by cellular precipitation as well as by the formation of modulated structures has been documented. The directions of modulations can be rationalized in terms of elastic strain energy considerations of the coherent precipitates. The shapes of the precipitates are also in accord with theoretical predictions. This report briefly describes the mechanisms of phase decomposition with particular emphasis on the role of elastic strain energy, the work on electron microscopic examination of modulated structures, and results of creep studies. 9 refs., 7 figs.

Research Organization:
Utah Univ., Salt Lake City, UT (USA). Dept. of Materials Science and Engineering
Sponsoring Organization:
USDOE; USDOE, Washington, DC (USA)
DOE Contract Number:
FG02-87ER45286
OSTI ID:
5554507
Report Number(s):
DOE/ER/45286-4; ON: DE91013296
Country of Publication:
United States
Language:
English