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Title: Microstructure evolution and tensile properties of Zr-2.5 wt.% Nb pressure tubes processed from billets with different microstructures

Journal Article · · Journal of Materials Engineering and Performance
;  [1];  [2]
  1. NDT, Hyderabad (India). Quality Assurance Group
  2. Defense Metallurgical Research Lab., Hyderabad (India)

Pressurized heavy water reactors (PHWR) use zirconium-base alloys for their low neutron-absorption cross section, good mechanical strength, low irradiation creep, and high corrosion resistance in reactor atmospheres. Starting with identical ingots, billets having different microstructures were obtained by three different processing methods for fabrication of Zr-2.5 wt%Nb pressure tubes., The billets were further processed by hot extrusion and cold Pilger tube reducing to the finished product. Microstructural characterization was done at each stage of processing. The effects of the initial billet microstructure on the intermediate and final microstructure and mechanical property results were determined. It was found that the structure at each stage and the final mechanical properties depend strongly on the initial billet microstructure. The structure at the final stage consists of elongated alpha zirconium grains with a network of metastable beta zirconium phase. Some of this metastable phase transforms into stable beta niobium during thermomechanical processing. Billets with quenched structure resulted in less beta niobium at the final stage. The air cooled billets resulted in a large amount of beta niobium. The tensile properties, especially the percentage elongation, were found to vary for the different methods. Higher percentage elongation was observed for billets having quenched structure. Extrusion and forging did not produce any characteristic differences in the properties. The results were used to select a process flow sheet which yields the desired mechanical properties with suitable microstructure in the final product.

OSTI ID:
335269
Journal Information:
Journal of Materials Engineering and Performance, Vol. 8, Issue 1; Other Information: PBD: Feb 1999
Country of Publication:
United States
Language:
English