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Title: Pressure, stress, and strain distribution in the double-stage diamond anvil cell

Journal Article · · Journal of Applied Physics
DOI:https://doi.org/10.1063/1.4927213· OSTI ID:22489538
;  [1]; ;  [2];  [3];  [4];  [3]
  1. Center for Advanced Radiation Sources, University of Chicago, Chicago, Illinois 60632 (United States)
  2. Photon Science DESY, D-22607 Hamburg (Germany)
  3. Geophysical Laboratory, Carnegie Institution of Washington, Washington, District of Columbia 20015 (United States)
  4. Key Laboratory of Earth and Planetary Physics, Institute of Geology and Geophysics CAS, Beijing 100029 (China)

Double stage diamond anvil cells (DACs) of two designs have been assembled and tested. We used a standard symmetric DAC with flat or beveled culets as a primary stage and CVD microanvils machined by a focused ion beam as a second. We evaluated pressure, stress, and strain distributions in gold and a mixture of gold and iron as well as in secondary anvils using synchrotron x-ray diffraction with a micro-focused beam. A maximum pressure of 240 GPa was reached independent of the first stage anvil culet size. We found that the stress field generated by the second stage anvils is typical of conventional DAC experiments. The maximum pressures reached are limited by strains developing in the secondary anvil and by cupping of the first stage diamond anvil in the presented experimental designs. Also, our experiments show that pressures of several megabars may be reached without sacrificing the first stage diamond anvils.

OSTI ID:
22489538
Journal Information:
Journal of Applied Physics, Vol. 118, Issue 3; Other Information: (c) 2015 AIP Publishing LLC; Country of input: International Atomic Energy Agency (IAEA); ISSN 0021-8979
Country of Publication:
United States
Language:
English

Cited By (6)

Toroidal diamond anvil cell for detailed measurements under extreme static pressures journal July 2018
Rapid Growth of Nanocrystalline Diamond on Single Crystal Diamond for Studies on Materials under Extreme Conditions journal January 2018
High pressure generation using double-stage diamond anvil technique: problems and equations of state of rhenium journal March 2018
Terapascal static pressure generation with ultrahigh yield strength nanodiamond journal July 2016
Terapascal static pressure generation with ultrahigh yield strength nanodiamond text January 2016
A perspective on conventional high-temperature superconductors at high pressure: Methods and materials journal April 2020