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Title: Magnetic properties of Nd-Ga-Fe{sub bal}-Nb-B alloy

Journal Article · · Journal of Applied Physics
DOI:https://doi.org/10.1063/1.4868602· OSTI ID:22273743
; ; ;  [1]
  1. Corporate R and D, Samsung Electro-Mechanics, Suwon (Korea, Republic of)

Here, we have synthesized Nd-Ga-Fe{sub bal}-Nb-B alloy by strip casting method. The crystalline and magnetic properties of sample were investigated with x-ray diffractometer (XRD), vibrating sample magnetometer (VSM), and Mössbauer spectrometer. The XRD pattern was analyzed with the Rietveld refinement method, indicating a tetragonal structure and the space group of P4{sub 2}/mnm. The temperature dependence of zero-field cooled (ZFC) magnetization curve was measured under applied field at temperature ranging from 4.2 to 740 K. From the ZFC curve, Curie temperature and spin reorientation temperature are determined to be 615 K and 130 K, respectively. Also, Mössbauer spectra were measured at various temperatures ranging from 4.2 to 620 K. Each spectrum was fitted with 6-sextets for Fe site (8j{sub 1}, 8j{sub 2}, 16k{sub 1}, 16k{sub 2}, 4c, and 4e), and magnetic hyperfine field, Isomer shift, electric quadrupole shift, and area ratio values were obtained from the fit. We observed the change in slope of magnetic hyperfine field and electric quadrupole shift at 130 K while the Curie temperature was determined to be 615 K from the measurement of zero velocity counter, agreeing with the values obtained from VSM measurements.

OSTI ID:
22273743
Journal Information:
Journal of Applied Physics, Vol. 115, Issue 17; Conference: 55. annual conference on magnetism and magnetic materials, Atlanta, GA (United States), 14-18 Nov 2010; Other Information: (c) 2014 AIP Publishing LLC; Country of input: International Atomic Energy Agency (IAEA); ISSN 0021-8979
Country of Publication:
United States
Language:
English