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Title: Determination of the structural changes by Raman and {sup 13}C CP/MAS NMR spectroscopy on native corn starch with plasticizers

Abstract

The plasticizing - antiplasticizing effect of water and glycerol contents on native corn starch samples is investigated by FT-Raman and {sup 13}C CP/MAS NMR spectroscopy. The presence of both amorphous and crystalline structural phases was evidenced in pure native corn starch and also in the samples containing plasticizers. Among the crystalline starch structures, the A- and V- types were suggested by CP/MAS NMR spectra.

Authors:
 [1]; ;  [2]; ; ;  [3]
  1. Academy of Romanian Scientists, Splaiul Independentei 54, 050094, Bucharest, Romania and National Institute of Research-Development for Machines and Installations Designed to Agriculture and Food Industry - INMA Bucureşti - Cluj-Napoca Branch (Romania)
  2. National Institute for Research and Development of Isotopic and Molecular Technologies, 65-103 Donath, 400293 Cluj-Napoca (Romania)
  3. National Institute of Research-Development for Machines and Installations Designed to Agriculture and Food Industry - INMA Bucureşti - Cluj-Napoca Branch, RO-400458 Cluj-Napoca (Romania)
Publication Date:
OSTI Identifier:
22257198
Resource Type:
Journal Article
Journal Name:
AIP Conference Proceedings
Additional Journal Information:
Journal Volume: 1565; Journal Issue: 1; Conference: PIM 2013: International conference on processes in isotopes and molecules, Cluj Napoca (Romania), 25-27 Sep 2013; Other Information: (c) 2013 AIP Publishing LLC; Country of input: International Atomic Energy Agency (IAEA); Journal ID: ISSN 0094-243X
Country of Publication:
United States
Language:
English
Subject:
37 INORGANIC, ORGANIC, PHYSICAL AND ANALYTICAL CHEMISTRY; GLYCEROL; NMR SPECTRA; NUCLEAR MAGNETIC RESONANCE; PLASTICIZERS; SPECTROSCOPY; STARCH

Citation Formats

Cozar, O., Filip, C., Tripon, C., Cioica, N., Coţa, C., and Nagy, E. M. Determination of the structural changes by Raman and {sup 13}C CP/MAS NMR spectroscopy on native corn starch with plasticizers. United States: N. p., 2013. Web. doi:10.1063/1.4833692.
Cozar, O., Filip, C., Tripon, C., Cioica, N., Coţa, C., & Nagy, E. M. Determination of the structural changes by Raman and {sup 13}C CP/MAS NMR spectroscopy on native corn starch with plasticizers. United States. https://doi.org/10.1063/1.4833692
Cozar, O., Filip, C., Tripon, C., Cioica, N., Coţa, C., and Nagy, E. M. 2013. "Determination of the structural changes by Raman and {sup 13}C CP/MAS NMR spectroscopy on native corn starch with plasticizers". United States. https://doi.org/10.1063/1.4833692.
@article{osti_22257198,
title = {Determination of the structural changes by Raman and {sup 13}C CP/MAS NMR spectroscopy on native corn starch with plasticizers},
author = {Cozar, O. and Filip, C. and Tripon, C. and Cioica, N. and Coţa, C. and Nagy, E. M.},
abstractNote = {The plasticizing - antiplasticizing effect of water and glycerol contents on native corn starch samples is investigated by FT-Raman and {sup 13}C CP/MAS NMR spectroscopy. The presence of both amorphous and crystalline structural phases was evidenced in pure native corn starch and also in the samples containing plasticizers. Among the crystalline starch structures, the A- and V- types were suggested by CP/MAS NMR spectra.},
doi = {10.1063/1.4833692},
url = {https://www.osti.gov/biblio/22257198}, journal = {AIP Conference Proceedings},
issn = {0094-243X},
number = 1,
volume = 1565,
place = {United States},
year = {Wed Nov 13 00:00:00 EST 2013},
month = {Wed Nov 13 00:00:00 EST 2013}
}