Cd–cysteine precursor nanowire templated microwave-assisted transformation route to CdS nanotubes

Liu, Xiao-Lin; Zhu, Ying-Jie; Zhang, Qian; Li, Zhi-Feng; Yang, Bin

doi:10.1016/J.MATERRESBULL.2012.09.021

Title: Cd–cysteine precursor nanowire templated microwave-assisted transformation route to CdS nanotubes

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Abstract

Graphical abstract: Cadmium sulfide polycrystalline nanotubes have been successfully synthesized by microwave-assisted transformation method using Cd–cysteine precursor nanowires as the source material and template in ethylene glycol at 160 °C or ethanol at 60 °C. Display Omitted Highlights: ► Cd–cysteine precursor nanowires were successfully synthesized in alkaline solution. ► CdS nanotubes were prepared by templated microwave-assisted transformation method. ► CdS nanotubes can well duplicate the size and morphology of precursor nanowires. ► This method has the advantages of the simplicity and low cost. -- Abstract: We report the Cd–cysteine precursor nanowire templated microwave-assisted transformation route to CdS nanotubes. In this method, the Cd–cysteine precursor nanowires are synthesized using CdCl{sub 2}·2.5H{sub 2}O, L-cysteine and ethanolamine in water at room temperature. The Cd–cysteine precursor nanowires are used as the source material and template for the subsequent preparation of CdS nanotubes by a microwave-assisted transformation method using ethylene glycol or ethanol as the solvent. This method has the advantages of the simplicity and low cost, and may be extended to the synthesis of nanotubes of other compounds. The products are characterized by X-ray powder diffraction (XRD), scanning electron microscopy (SEM) and transmission electron microscopy (TEM).

Authors:

Liu, Xiao-Lin ^[1]; Zhu, Ying-Jie ^[2]; Zhang, Qian; Li, Zhi-Feng; Yang, Bin ^[1]

School of Material Science and Engineering, Jiangxi University of Science and Technology, Ganzhou 341000 (China)
State Key Laboratory of High Performance Ceramics and Superfine Microstructure, Shanghai Institute of Ceramics, Chinese Academy of Sciences, Shanghai 200050 (China)

Publication Date:: Sat Dec 15 00:00:00 EST 2012

OSTI Identifier:: 22215673

Resource Type:: Journal Article

Journal Name:: Materials Research Bulletin

Additional Journal Information:: Journal Volume: 47; Journal Issue: 12; Other Information: Copyright (c) 2012 Elsevier Science B.V., Amsterdam, The Netherlands, All rights reserved.; Country of input: International Atomic Energy Agency (IAEA); Journal ID: ISSN 0025-5408

Country of Publication:: United States

Language:: English

Subject:: 77 NANOSCIENCE AND NANOTECHNOLOGY; 36 MATERIALS SCIENCE; CADMIUM SULFIDES; CYSTEINE; GLYCOLS; MICROSTRUCTURE; NANOTUBES; POLYCRYSTALS; PRECURSOR; QUANTUM WIRES; SCANNING ELECTRON MICROSCOPY; SYNTHESIS; TRANSMISSION ELECTRON MICROSCOPY; X-RAY DIFFRACTION

Citation Formats


                    Liu, Xiao-Lin, Zhu, Ying-Jie, Zhang, Qian, Li, Zhi-Feng, and Yang, Bin. Cd–cysteine precursor nanowire templated microwave-assisted transformation route to CdS nanotubes.  United States: N. p., 2012. 
        Web.  doi:10.1016/J.MATERRESBULL.2012.09.021.

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                    Liu, Xiao-Lin, Zhu, Ying-Jie, Zhang, Qian, Li, Zhi-Feng, & Yang, Bin. Cd–cysteine precursor nanowire templated microwave-assisted transformation route to CdS nanotubes.  United States.  https://doi.org/10.1016/J.MATERRESBULL.2012.09.021

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                    Liu, Xiao-Lin, Zhu, Ying-Jie, Zhang, Qian, Li, Zhi-Feng, and Yang, Bin. 2012.  
        "Cd–cysteine precursor nanowire templated microwave-assisted transformation route to CdS nanotubes".  United States.  https://doi.org/10.1016/J.MATERRESBULL.2012.09.021.

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@article{osti_22215673,

  title        = {Cd–cysteine precursor nanowire templated microwave-assisted transformation route to CdS nanotubes},

  author       = {Liu, Xiao-Lin and Zhu, Ying-Jie and Zhang, Qian and Li, Zhi-Feng and Yang, Bin},

  abstractNote = {Graphical abstract: Cadmium sulfide polycrystalline nanotubes have been successfully synthesized by microwave-assisted transformation method using Cd–cysteine precursor nanowires as the source material and template in ethylene glycol at 160 °C or ethanol at 60 °C. Display Omitted Highlights: ► Cd–cysteine precursor nanowires were successfully synthesized in alkaline solution. ► CdS nanotubes were prepared by templated microwave-assisted transformation method. ► CdS nanotubes can well duplicate the size and morphology of precursor nanowires. ► This method has the advantages of the simplicity and low cost. -- Abstract: We report the Cd–cysteine precursor nanowire templated microwave-assisted transformation route to CdS nanotubes. In this method, the Cd–cysteine precursor nanowires are synthesized using CdCl{sub 2}·2.5H{sub 2}O, L-cysteine and ethanolamine in water at room temperature. The Cd–cysteine precursor nanowires are used as the source material and template for the subsequent preparation of CdS nanotubes by a microwave-assisted transformation method using ethylene glycol or ethanol as the solvent. This method has the advantages of the simplicity and low cost, and may be extended to the synthesis of nanotubes of other compounds. The products are characterized by X-ray powder diffraction (XRD), scanning electron microscopy (SEM) and transmission electron microscopy (TEM).},

  doi          = {10.1016/J.MATERRESBULL.2012.09.021},

  url          = {https://www.osti.gov/biblio/22215673},
  journal      = {Materials Research Bulletin},

  issn         = {0025-5408},

  number       = 12,

  volume       = 47,

  place        = {United States},

  year         = {Sat Dec 15 00:00:00 EST 2012},

  month        = {Sat Dec 15 00:00:00 EST 2012}

}

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