Spectroscopic studies and crystal structure of (E)-N Prime -(2-hydroxy-3-methoxybenzylidene)isonicotinohydrazide

Journal Article · Tue Jan 15 00:00:00 EST 2013 · Crystallography Reports

DOI:https://doi.org/10.1134/S1063774513010264· OSTI ID:22156466

Yildiz, M. ^[1]; Unver, H. ^[2]; Kiraz, A. ^[3]

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1. Canakkaale Onsekiz Mart University, Department of Chemistry, Faculty of Science and Arts (Turkey)
2. Ankara University, Department of Physics, Faculty of Science (Turkey)
3. Near East University, Ataturk Faculty of Education (Turkey)

The structure of compound has also been examined cyrstallographically. It crystallizes in the monoclinic space group P2{sub 1}/c with a = 7.673(1), b = 16.251(2), c = 10.874(1) A, {beta} = 110.42(1) Degree-Sign , V = 1270.7(3) A{sup 3}, D{sub x} = 1.418 g cm{sup -3}, R{sub 1} = 0.0349 and wR{sub 2} = 0.0935 [I > 2{sigma}(I)], respectively. The title compound has been synthesized from the reaction of isonicotinohydrazide with 2-hydroxy-3-methoxybenzaldehyde. It has been characterized by using elemental analysis, MS, IR, {sup 1}H NMR, {sup 13}C NMR and UV-Visible spectroscopic techniques.

• OSTI ID: 22156466
• Journal Information: Crystallography Reports, Vol. 58, Issue 1; Other Information: Copyright (c) 2013 Pleiades Publishing, Ltd.; Country of input: International Atomic Energy Agency (IAEA); ISSN 1063-7745
• Country of Publication: United States
• Language: English

Related Subjects

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MONOCLINIC LATTICES
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SPACE GROUPS