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Title: Preparation of W-Ta thin-film thermocouple on diamond anvil cell for in-situ temperature measurement under high pressure

Journal Article · · Review of Scientific Instruments
DOI:https://doi.org/10.1063/1.3579515· OSTI ID:22062305
 [1];  [2]; ;  [1]
  1. State Key Laboratory for Superhard Materials, Institute of Atomic and Molecular Physics, Jilin University, Changchun 130012 (China)
  2. College of Physics and Chemistry, Henan Polytechnic University, Jiaozuo 454000 (China)

In this paper, a W-Ta thin-film thermocouple has been integrated on a diamond anvil cell by thin-film deposition and photolithography methods. The thermocouple was calibrated and its thermal electromotive force was studied under high pressure. The results indicate that the thermal electromotive force of the thermocouple exhibits a linear relationship with temperature and is not associated with pressure. The resistivity measurement of ZnS powders under high pressure at different temperatures shows that the phase transition pressure decreases as the temperature increases.

OSTI ID:
22062305
Journal Information:
Review of Scientific Instruments, Vol. 82, Issue 4; Other Information: (c) 2011 American Institute of Physics; Country of input: International Atomic Energy Agency (IAEA); ISSN 0034-6748
Country of Publication:
United States
Language:
English