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Title: Non-destructive testing of satellite nozzles made of carbon fibre ceramic matrix composite, C/SiC

Journal Article · · Materials Characterization
 [1];  [2]
  1. Technische Universitaet Muenchen, ZWE, FRM-II, Forschungsneutronenquelle Heinz Maier-Leibnitz, Lichtenbergstr. 1, D-85747 Garching (Germany)
  2. EADS-Space-Transportation, Willy-Messerschmitt-Str.D-85521 Munich (Germany)

Carbon fibre ceramic matrix composite materials, C/SiC, are excellent candidates as lightweight structural materials for high performance hot structures such as in aerospace applications. Satellite nozzles are manufactured from C/SiC, using, for instance, the Liquid Polymer Infiltration (LPI) process. In this article the applicability of different non-destructive analysis methods for the characterisation of C/SiC components will be discussed. By using synchrotron and neutron tomography it is possible to characterise the C/SiC material in each desired location or orientation. Synchrotron radiation using tomography on small samples with a resolution of 1.4 {mu}m, i.e. the fibre scale, was used to characterise three dimensionally fibre orientation and integrity, matrix homogeneity and dimensions and distributions of micro pores. Neutron radiation tomography with a resolution of about 300 {mu}m was used to analyse the over-all C/SiC satellite nozzle component with respect to the fibre content. The special solder connection of a C/SiC satellite nozzle to a metallic ring was also successfully analysed by neutron tomography. In addition, the residual stress state of a temperature tested satellite nozzle was analysed non-destructively in depth by neutron diffraction. The results revealed almost zero stress for the principal directions, radial, axial and tangential, which can be considered to be the principal directions.

OSTI ID:
21062159
Journal Information:
Materials Characterization, Vol. 58, Issue 10; Other Information: DOI: 10.1016/j.matchar.2006.09.010; PII: S1044-5803(06)00275-0; Copyright (c) 2006 Elsevier Science B.V., Amsterdam, The Netherlands, All rights reserved; Country of input: International Atomic Energy Agency (IAEA); ISSN 1044-5803
Country of Publication:
United States
Language:
English