Quantitative mineralogical analysis of hydraulic limes by X-ray diffraction

Journal Article · Thu Nov 15 00:00:00 EST 2007 · Cement and Concrete Research

DOI:https://doi.org/10.1016/j.cemconres.2007.08.002· OSTI ID:21033050

Madau, P ^[1]; Durinck, D; Blanpain, B ^[2]; Elsen, J ^[3]

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1. Chimie Industrielle, Universite Libre de Bruxelles, avenue F.D. Roosevelt 50, 1050 Brussels (Belgium)
2. MTM, Katholieke Universiteit Leuven, Kasteelpark 44, 3001 Heverlee (Belgium)
3. Fysico-chemische Geologie, Katholieke Universiteit Leuven, Celestijnenlaan 200E, 3001 Heverlee (Belgium)

A combined selective dissolution/quantitative X-ray diffraction (QXRD) approach is proposed for the quantitative mineralogical phase analysis of hydraulic limes. The proposed methodology is validated by the analysis of two model mixtures. Afterwards two commercial hydraulic binders and one self-burned hydraulic quicklime were analysed. Chemical, thermal and microprobe analyses were performed to check the results. It is shown that the proposed selective dissolution/QXRD approach yields reliable quantitative mineralogical information for hydraulic limes in spite of their complex phase composition and the presence of amorphous material.

• OSTI ID: 21033050
• Journal Information: Cement and Concrete Research, Vol. 37, Issue 11; Other Information: DOI: 10.1016/j.cemconres.2007.08.002; PII: S0008-8846(07)00167-6; Copyright (c) 2007 Elsevier Science B.V., Amsterdam, The Netherlands, All rights reserved; Country of input: International Atomic Energy Agency (IAEA); ISSN 0008-8846
• Country of Publication: United States
• Language: English

Related Subjects

36 MATERIALS SCIENCE
BINDERS
CLAYS
DISSOLUTION
LIMESTONE
MIXTURES
MORTARS
PHASE STUDIES
THERMAL ANALYSIS
X-RAY DIFFRACTION