Six-circle diffractometer with atmosphere- and temperature-controlled sample stage and area and line detectors for use in the G2 experimental station at CHESS

Journal Article · Wed Nov 15 00:00:00 EST 2006 · Review of Scientific Instruments

DOI:https://doi.org/10.1063/1.2372730· OSTI ID:20861492

Nowak, D E; Blasini, D R; Vodnick, A M; Blank, B; Tate, M W; Deyhim, A; Smilgies, D -M; Abruna, H; Gruner, S M; Baker, S P ^[1]

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1. Department of Materials Science and Engineering, Cornell University, Ithaca, New York 14853 (United States)

A new diffractometer system was designed and built for the G2 experimental station at the Cornell High Energy Synchrotron Source (CHESS). A six-circle {kappa} goniometer, which provides better access to reciprocal space compared to Eulerian cradles, was chosen primarily to perform large angle Bragg diffraction on samples with preferred crystallographic orientations, and can access both horizontal and vertical diffraction planes. A new atmosphere- and temperature-controlled sample stage was designed for thin film thermomechanical experiments. The stage can be operated in ultrahigh vacuum and uses a Be dome x-ray window to provide access to all scattering vectors above a sample's horizon. A novel design minimizes sample displacements during thermal cycling to less than 160 {mu}m over 900 deg. C and the stage is motorized for easy height adjustments, which can be used to compensate for displacements from thermal expansion. A new area detector was built and a new line detector was purchased. Both detectors cover a large region in reciprocal space, providing the ability to measure time-resolved phenomena. A detailed description of the design and technical characteristics is given. Some capabilities of the diffractometer system are illustrated by a strain analysis on a thin metal film and characterization of organic thin films with grazing incidence diffraction. The G2 experimental station, as part of CHESS, is a national user facility and is available to external users by application.

• OSTI ID: 20861492
• Journal Information: Review of Scientific Instruments, Vol. 77, Issue 11; Other Information: DOI: 10.1063/1.2372730; (c) 2006 American Institute of Physics; Country of input: International Atomic Energy Agency (IAEA); ISSN 0034-6748
• Country of Publication: United States
• Language: English

Related Subjects

46 INSTRUMENTATION RELATED TO NUCLEAR SCIENCE AND TECHNOLOGY
36 MATERIALS SCIENCE
BRAGG REFLECTION
CRYSTALLOGRAPHY
CRYSTALS
DESIGN
DIFFRACTION
GONIOMETERS
HEIGHT
METALS
ORGANIC COMPOUNDS
ORIENTATION
STRAINS
SYNCHROTRON RADIATION SOURCES
THERMAL CYCLING
THERMAL EXPANSION
THIN FILMS
TIME RESOLUTION
X RADIATION
X-RAY DIFFRACTOMETERS