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Title: Three-Dimensional GaN-Ga{sub 2}O{sub 3} Core Shell Structure Revealed by X-Ray Diffraction Microscopy

Journal Article · · Physical Review Letters
; ;  [1]; ;  [2]; ; ;  [3];  [4]
  1. Department of Physics and Astronomy and California NanoSystems Institute, University of California, Los Angeles, California 90095 (United States)
  2. Institute of Physics, Academia Sinica, Nankang, Taipei, 11529, Taiwan (China)
  3. SPring-8/RIKEN, 1-1-1, Kouto, Mikazuki, Sayo-gun, Hyogo 679-5198 (Japan)
  4. Department of Chemical Engineering and Materials Science, University of California, Davis, California 95616 (United States)

In combination of direct phase retrieval of coherent x-ray diffraction patterns with a novel tomographic reconstruction algorithm, we, for the first time, carried out quantitative 3D imaging of a heat-treated GaN particle with each voxel corresponding to 17x17x17 nm{sup 3}. We observed the platelet structure of GaN and the formation of small islands on the surface of the platelets, and successfully captured the internal GaN-Ga{sub 2}O{sub 3} core shell structure in three dimensions. This work opens the door for nondestructive and quantitative imaging of 3D morphology and 3D internal structure of a wide range of materials at the nanometer scale resolution that are amorphous or possess only short-range atomic organization.

OSTI ID:
20861402
Journal Information:
Physical Review Letters, Vol. 97, Issue 21; Other Information: DOI: 10.1103/PhysRevLett.97.215503; (c) 2006 The American Physical Society; Country of input: International Atomic Energy Agency (IAEA); ISSN 0031-9007
Country of Publication:
United States
Language:
English