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Title: Granulation of fine powder

Patent ·
OSTI ID:1289917

A mixture of fine powder including thorium oxide was converted to granulated powder by forming a first-green-body and heat treating the first-green-body at a high temperature to strengthen the first-green-body followed by granulation by crushing or milling the heat-treated first-green-body. The granulated powder was achieved by screening through a combination of sieves to achieve the desired granule size distribution. The granulated powder relies on the thermal bonding to maintain its shape and structure. The granulated powder contains no organic binder and can be stored in a radioactive or other extreme environment. The granulated powder was pressed and sintered to form a dense compact with a higher density and more uniform pore size distribution.

Research Organization:
Los Alamos National Laboratory (LANL), Los Alamos, NM (United States)
Sponsoring Organization:
USDOE
DOE Contract Number:
AC52-06NA25396
Assignee:
Los Alamos National Security, LLC (Los Alamos, NM)
Patent Number(s):
9,409,825
Application Number:
13/971,157
OSTI ID:
1289917
Resource Relation:
Patent File Date: 2013 Aug 20
Country of Publication:
United States
Language:
English

References (23)

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Method of producing PuO.sub.2 /UO.sub.2 /-nuclear fuels patent January 1981
Reactor and process for production of novel nuclear fuel patent April 1983
Method for producing nuclear fuel patent May 1983
Method of improving the green strength of nuclear fuel pellets patent May 1983
Fugitive binder-containing nuclear fuel material and method of production patent June 1983
Method for producing nuclear fuel pellets, and product thereof patent February 1984
Process for the manufacture of fine propellant powders by granulation, and powders thus obtained patent April 1984
Polymeric binders for enhancing green strength of pressed ceramics patent January 1996
Ceramic granules, process for preparing the same, and process for producing sintered product of silicon nitride patent May 1999
Ceramic composition for immobilization of actinides patent October 2000
Process for making a ceramic composition for immobilization of actinides patent November 2001
Process for producing granules for being molded into ferrite, granules for being molded into ferrite, green body and sintered body patent February 2005
Method for manufacturing spherical ceramic powder patent July 2008
Method for making product from fiber glass waste patent August 2008
Thermal spray feedstock composition patent September 2010
Method for producing raw material powder for rare earth sintered magnet, method for producing rare earth sintered magnet, granule and sintered body patent December 2010
Granulating fine powders into millimetric spheres with a multiscale porosity: The case of titania journal April 2011
Critical parameters and limiting conditions in binder granulation of fine powders journal December 1997
Microgranulation of fine powders by a novel rotating fluidized bed granulator journal April 2003

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