High gain durable anti-reflective coating

Maghsoodi, Sina; Brophy, Brenor L.; Colson, Thomas E.; Gonsalves, Peter R.; Abrams, Ze'ev R.

Title: High gain durable anti-reflective coating

Patent · Tue Jul 26 00:00:00 EDT 2016

OSTI ID:1273457

Maghsoodi, Sina; Brophy, Brenor L.; Colson, Thomas E.; Gonsalves, Peter R.; Abrams, Ze'ev R.

Disclosed herein are polysilsesquioxane-based anti-reflective coating (ARC) compositions, methods of preparation, and methods of deposition on a substrate. In one embodiment, the polysilsesquioxane of this disclosure is prepared in a two-step process of acid catalyzed hydrolysis of organoalkoxysilane followed by addition of tetralkoxysilane that generates silicone polymers with >40 mol % silanol based on Si-NMR. These high silanol siloxane polymers are stable and have a long shelf-life in polar organic solvents at room temperature. Also disclosed are low refractive index ARC made from these compositions with and without additives such as porogens, templates, thermal radical initiator, photo radical initiators, crosslinkers, Si--OH condensation catalyst and nano-fillers. Also disclosed are methods and apparatus for applying coatings to flat substrates including substrate pre-treatment processes, coating processes and coating curing processes including skin-curing using hot-air knives. Also disclosed are coating compositions and formulations for highly tunable, durable, highly abrasion-resistant functionalized anti-reflective coatings.

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Research Organization:: Enki Technology, Inc., San Jose, CA (United States)

Sponsoring Organization:: USDOE

DOE Contract Number:: EE0006810

Assignee:: Enki Technology, Inc. (San Jose, CA)

Patent Number(s):: 9,399,720

Application Number:: 14/799,507

OSTI ID:: 1273457

Resource Relation:: Patent File Date: 2015 Jul 14

Country of Publication:: United States

Language:: English

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Mass Production of PV Modules with 18% Total-Area Efficiency and High Energy Delivery Per Peak Watt Rose, Doug; Koehler, Oliver; Kaminar, Neil 2006 IEEE 4th World Conference on Photovoltaic Energy Conference https://doi.org/10.1109/WCPEC.2006.279898	conference	May 2006
A highly abrasive-resistant, long-lasting anti-reflective coating for PV module glass Pop, Sergiu C.; Abbaraju, Venkata; Brophy, Brenor 2014 IEEE 40th Photovoltaic Specialists Conference (PVSC), 2014 IEEE 40th Photovoltaic Specialist Conference (PVSC) https://doi.org/10.1109/PVSC.2014.6925490	conference	June 2014
Long-term durability of sol–gel porous coatings for solar glass covers San Vicente, G.; Bayón, R.; Germán, N. Thin Solid Films, Vol. 517, Issue 10, p. 3157-3160 https://doi.org/10.1016/j.tsf.2008.11.079	journal	March 2009
Surface modification of porous antireflective coatings for solar glass covers San Vicente, G.; Bayón, R.; Germán, N. Solar Energy, Vol. 85, Issue 4, p. 676-680 https://doi.org/10.1016/j.solener.2010.06.009	journal	April 2011
Laboratory study of potential induced degradation of silicon photovoltaic modules Schutze, M.; Junghanel, M.; Koentopp, M. B. 2011 37th IEEE Photovoltaic Specialists Conference (PVSC) https://doi.org/10.1109/PVSC.2011.6186080	conference	June 2011
Potential induced degradation of pre-stressed photovoltaic modules: Effect of glass surface conductivity disruption Tatapudi, S.; Ebneali, F.; Kuitche, J. 2013 IEEE 39th Photovoltaic Specialists Conference (PVSC) https://doi.org/10.1109/PVSC.2013.6744452	conference	June 2013
Comparative study on hydrophobic anti-reflective films from three kinds of methyl-modified silica sols Xu, Yao; Wu, Dong; Sun, Yu Han Journal of Non-Crystalline Solids, Vol. 351, Issue 3, p. 258-266 https://doi.org/10.1016/j.jnoncrysol.2004.11.011	journal	February 2005
Durable solgel antireflective films with high laser-induced damage thresholds for inertial confinement fusion Xu, Yao; Zhang, Lei; Wu, Dong Journal of the Optical Society of America B, Vol. 22, Issue 4 https://doi.org/10.1364/JOSAB.22.000905	journal	January 2005
SiO2 as barrier layer for Na out-diffusion from soda-lime glass Yan, Yanfa; Li, Xiaonan; Dhere, Ramesh 2010 35th IEEE Photovoltaic Specialists Conference (PVSC) https://doi.org/10.1109/PVSC.2010.5614657	conference	June 2010

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