Surface sampling concentration and reaction probe with controller to adjust sampling position

Van Berkel, Gary J.; ElNaggar, Mariam S.

Title: Surface sampling concentration and reaction probe with controller to adjust sampling position

Patent · Tue Jul 19 00:00:00 EDT 2016

OSTI ID:1264416

Van Berkel, Gary J.; ElNaggar, Mariam S.

A method of analyzing a chemical composition of a specimen is described. The method can include providing a probe comprising an outer capillary tube and an inner capillary tube disposed co-axially within the outer capillary tube, where the inner and outer capillary tubes define a solvent capillary and a sampling capillary in fluid communication with one another at a distal end of the probe; contacting a target site on a surface of a specimen with a solvent in fluid communication with the probe; maintaining a plug volume proximate a solvent-specimen interface, wherein the plug volume is in fluid communication with the probe; draining plug sampling fluid from the plug volume through the sampling capillary; and analyzing a chemical composition of the plug sampling fluid with an analytical instrument. A system for performing the method is also described.

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Research Organization:: Oak Ridge National Laboratory (ORNL), Oak Ridge, TN (United States)

Sponsoring Organization:: USDOE

DOE Contract Number:: AC05-00OR22725

Assignee:: UT-BATTELLE, LLC (Oak Ridge, TN)

Patent Number(s):: 9,395,278

Application Number:: 13/936,715

OSTI ID:: 1264416

Resource Relation:: Patent File Date: 2013 Jul 08

Country of Publication:: United States

Language:: English

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