Highly compressible 3D periodic graphene aerogel microlattices

Zhu, Cheng; Han, T. Yong-Jin; Duoss, Eric B.; Golobic, Alexandra M.; Kuntz, Joshua D.; Spadaccini, Christopher M.; Worsley, Marcus A.

doi:10.1038/ncomms7962

Title: Highly compressible 3D periodic graphene aerogel microlattices

Journal Article · Wed Apr 22 00:00:00 EDT 2015 · Nature Communications

DOI:https://doi.org/10.1038/ncomms7962· OSTI ID:1259507

Zhu, Cheng ^[1]; Han, T. Yong-Jin ^[1]; Duoss, Eric B. ^[1]; Golobic, Alexandra M. ^[1]; Kuntz, Joshua D. ^[1]; Spadaccini, Christopher M. ^[1];

^[1]

Lawrence Livermore National Lab. (LLNL), Livermore, CA (United States)

Graphene is a two-dimensional material that offers a unique combination of low density, exceptional mechanical properties, large surface area and excellent electrical conductivity. Recent progress has produced bulk 3D assemblies of graphene, such as graphene aerogels, but they possess purely stochastic porous networks, which limit their performance compared with the potential of an engineered architecture. Here we report the fabrication of periodic graphene aerogel microlattices, possessing an engineered architecture via a 3D printing technique known as direct ink writing. The 3D printed graphene aerogels are lightweight, highly conductive and exhibit supercompressibility (up to 90% compressive strain). Moreover, the Young’s moduli of the 3D printed graphene aerogels show an order of magnitude improvement over bulk graphene materials with comparable geometric density and possess large surface areas. Ultimately, adapting the 3D printing technique to graphene aerogels realizes the possibility of fabricating a myriad of complex aerogel architectures for a broad range of applications.

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Research Organization:: Lawrence Livermore National Laboratory (LLNL), Livermore, CA (United States)

Sponsoring Organization:: USDOE Laboratory Directed Research and Development (LDRD) Program

Grant/Contract Number:: AC52-07NA27344; 14-SI-004; 13-LW-099

OSTI ID:: 1259507

Alternate ID(s):: OSTI ID: 1410001

Report Number(s):: LLNL-JRNL-665510; ncomms7962

Journal Information:: Nature Communications, Vol. 6; ISSN 2041-1723

Publisher:: Nature Publishing GroupCopyright Statement

Country of Publication:: United States

Language:: English

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Cited by: 824 works

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Highly compressible and superior low temperature tolerant supercapacitors based on dual chemically crosslinked PVA hydrogel electrolytes Liu, Zhenzhen; Zhang, Junmei; Liu, Jing Journal of Materials Chemistry A, Vol. 8, Issue 13 https://doi.org/10.1039/c9ta12424a	journal	January 2020
Graphene aerogels: a review Gorgolis, George; Galiotis, Costas 2D Materials, Vol. 4, Issue 3 https://doi.org/10.1088/2053-1583/aa7883	journal	June 2017
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Recent Advances in 3D Graphene Architectures and Their Composites for Energy Storage Applications Wang, Zhijie; Gao, Hong; Zhang, Qing Small https://doi.org/10.1002/smll.201803858	journal	December 2018
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3D Printing of Free-Standing Stretchable Electrodes with Tunable Structure and Stretchability Wei, Hong; Li, Kai; Liu, Wen Guang Advanced Engineering Materials, Vol. 19, Issue 11 https://doi.org/10.1002/adem.201700341	journal	July 2017
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Direct Ink Write (DIW) 3D Printed Cellulose Nanocrystal Aerogel Structures Li, Vincent Chi-Fung; Dunn, Conner K.; Zhang, Zhe Scientific Reports, Vol. 7, Issue 1 https://doi.org/10.1038/s41598-017-07771-y	journal	August 2017
Fabrication of bagel-like graphene aerogels and its application in pressure sensors Li, Zongheng; Ning, Huiming; Liu, Liangbin Smart Materials and Structures, Vol. 28, Issue 5 https://doi.org/10.1088/1361-665x/ab0ea3	journal	April 2019
Mesoporous Li ₃ VO ₄ /C Submicron-Ellipsoids Supported on Reduced Graphene Oxide as Practical Anode for High-Power Lithium-Ion Batteries Li, Qidong; Wei, Qiulong; Sheng, Jinzhi Advanced Science, Vol. 2, Issue 12 https://doi.org/10.1002/advs.201500284	journal	October 2015
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Conductivity Maximum in 3D Graphene Foams Liu, Feng; Wang, Chao; Tang, Qiheng Small, Vol. 14, Issue 32 https://doi.org/10.1002/smll.201801458	journal	July 2018
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3D Printing of Highly Conductive Nanocomposites for the Functional Optimization of Liquid Sensors Chizari, Kambiz; Daoud, Mohamed Amine; Ravindran, Anil Raj Small, Vol. 12, Issue 44 https://doi.org/10.1002/smll.201601695	journal	September 2016
Understanding Mechanical Response of Elastomeric Graphene Networks Ni, Na; Barg, Suelen; Garcia-Tunon, Esther Scientific Reports, Vol. 5, Issue 1 https://doi.org/10.1038/srep13712	journal	September 2015
Three-dimensional nitrogen and phosphorus co-doped carbon quantum dots/reduced graphene oxide composite aerogels with a hierarchical porous structure as superior electrode materials for supercapacitors Li, Jingying; Yun, Xiaoru; Hu, Zhongliang Journal of Materials Chemistry A, Vol. 7, Issue 46 https://doi.org/10.1039/c9ta08151h	journal	January 2019
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The Emerging Frontiers and Applications of High-Resolution 3D Printing Mao, Mao; He, Jiankang; Li, Xiao Micromachines, Vol. 8, Issue 4 https://doi.org/10.3390/mi8040113	journal	April 2017
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High-quality graphene aerogels for thermally conductive phase change composites with excellent shape stability Yang, Jing; Li, Xiaofeng; Han, Shuang Journal of Materials Chemistry A, Vol. 6, Issue 14 https://doi.org/10.1039/c8ta00078f	journal	January 2018
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Active Mixing of Reactive Materials for 3D Printing Golobic, Alexandra M.; Durban, Matthew D.; Fisher, Scott E. Advanced Engineering Materials, Vol. 21, Issue 8 https://doi.org/10.1002/adem.201900147	journal	May 2019
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Extraordinary tensile strength and ductility of scalable nanoporous graphene Kashani, Hamzeh; Ito, Yoshikazu; Han, Jiuhui Science Advances, Vol. 5, Issue 2 https://doi.org/10.1126/sciadv.aat6951	journal	February 2019
Superelastic Hard Carbon Nanofiber Aerogels Yu, Zhi‐Long; Qin, Bing; Ma, Zhi‐Yuan Advanced Materials, Vol. 31, Issue 23 https://doi.org/10.1002/adma.201900651	journal	March 2019
Low-Density Open Cellular Sponges as Functional Materials Jiang, Shaohua; Agarwal, Seema; Greiner, Andreas Angewandte Chemie International Edition, Vol. 56, Issue 49 https://doi.org/10.1002/anie.201700684	journal	November 2017
Nanomaterials in Advanced, High-Performance Aerogel Composites: A Review Barrios, Elizabeth; Fox, David; Li Sip, Yuen Yee Polymers, Vol. 11, Issue 4 https://doi.org/10.3390/polym11040726	journal	April 2019
Compressible and conductive carbon aerogels from waste paper with exceptional performance for oil/water separation Li, Lingxiao; Li, Bucheng; Sun, Hanxue Journal of Materials Chemistry A, Vol. 5, Issue 28 https://doi.org/10.1039/c7ta03511j	journal	January 2017
Ring Shuttling Controls Macroscopic Motion in a Three-Dimensional Printed Polyrotaxane Monolith Lin, Qianming; Hou, Xisen; Ke, Chenfeng Angewandte Chemie International Edition, Vol. 56, Issue 16 https://doi.org/10.1002/anie.201612440	journal	March 2017
Assembly and Electronic Applications of Colloidal Nanomaterials Zhu, Jian; Hersam, Mark C. Advanced Materials, Vol. 29, Issue 4 https://doi.org/10.1002/adma.201603895	journal	November 2016
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Advances on Microsized On-Chip Lithium-Ion Batteries Liu, Lixiang; Weng, Qunhong; Lu, Xueyi Small, Vol. 13, Issue 45 https://doi.org/10.1002/smll.201701847	journal	September 2017
Ultralight shape-recovering plate mechanical metamaterials Davami, Keivan; Zhao, Lin; Lu, Eric Nature Communications, Vol. 6, Issue 1 https://doi.org/10.1038/ncomms10019	journal	December 2015
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Compressive Response of Non-slender Octet Carbon Microlattices Kudo, Akira; Misseroni, Diego; Wei, Yuchen Frontiers in Materials, Vol. 6 https://doi.org/10.3389/fmats.2019.00169	journal	July 2019
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